Benzenemethanamine, N-(1-methylethyl)-N-nitroso-

Base Information

• Chemical Name: Benzenemethanamine, N-(1-methylethyl)-N-nitroso-
• CAS No.: 20689-97-8
• Molecular Formula: C10H14N2O
• Molecular Weight: 178.234
• Mol file: 20689-97-8.mol

Synonyms:

Chemical Property of Benzenemethanamine, N-(1-methylethyl)-N-nitroso-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanamine, N-(1-methylethyl)-N-nitroso-

There total 2 articles about Benzenemethanamine, N-(1-methylethyl)-N-nitroso- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Benzyl-isopropyl-amin (102-97-6) → N-benzyl-N-isopropylnitrous amide (20689-97-8)

Guidance literature:

With N,N,N’,N’-tetrabromobenzene-1,3-disulfonamide; water; silica gel; sodium nitrite; In dichloromethane; at 20 ℃; for 0.05h; Reagent/catalyst;

DOI:10.2174/1570178611310030011

Reference yield:

→ N-benzyl-N-isopropylnitrous amide (20689-97-8)

Guidance literature:

Neben trans-Benzyl-isopropyl-nitrosamin;

Reference yield:

N-benzyl-N-isopropylnitrous amide (20689-97-8) → N-benzyl-N-isopropylnitrous amide (91010-23-0)

Guidance literature:

With acetic acid; zinc; In water; at 15 ℃; for 12h; Reflux; Inert atmosphere;

DOI:10.1002/anie.201209618

upstream raw materials:

Benzyl-isopropyl-amin

Downstream raw materials:

N-benzyl-N-isopropylnitrous amide

Refernces

• 1、 Ghorbani-Vaghei, Ramin,Shiri, Lotfi,Ghorbani-Choghamarani, Arash. "Facile N-nitrosation of secondary amines using poly(N,N'-dibromo-Nethylene- benzene-1,3-disulfonamide) and N,N,N′,N′-tetrabromobenzene-1,3- disulfonamide/NaNO2 under mild conditions". . p. 204 - 208. Retrieved 2013/07/26.