1,3,5-triethyl-2-iodobenzene

Base Information

• Chemical Name: 1,3,5-triethyl-2-iodobenzene
• CAS No.: 2100-21-2
• Molecular Formula: C12H17I
• Molecular Weight: 288.171
• Mol file: 2100-21-2.mol

Synonyms:

Chemical Property of 1,3,5-triethyl-2-iodobenzene

Chemical Property:

• Vapor Pressure: 0.00597mmHg at 25°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,5-triethyl-2-iodobenzene

There total 4 articles about 1,3,5-triethyl-2-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

1,3,5-triethylbenzene (102-25-0) → 2-iodo-1,3,5-triethylbenzene (2100-21-2)

Guidance literature:

With N-chloro-succinimide; sodium iodide; In acetic acid; at 100 ℃; for 12h;

DOI:10.1016/j.tetlet.2009.12.125

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 2-iodo-1,3,5-triethylbenzene (2100-21-2)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: iodic acid; glacial acetic acid; iodine

With aluminium trichloride; iodine; iodic acid; acetic acid;

Reference yield:

2-nitro-1,3,5-triethylbenzene (13402-30-7) → 2-iodo-1,3,5-triethylbenzene (2100-21-2)

Guidance literature:

Multi-step reaction with 2 steps

1: iron; water

2: Diazotization_.Behandlung der Diazoniumsalz-Loesung mit KI

With water; iron;

DOI:10.1021/ja01278a014

upstream raw materials:

1,3,5-triethylbenzene

2,4,6-triethylbenzenamine

2-nitro-1,3,5-triethylbenzene

benzene

Downstream raw materials:

2-nitro-1,3,5-triethylbenzene

Refernces