Cyclohexyl, 1-hydroxy-

Base Information

• Chemical Name: Cyclohexyl, 1-hydroxy-
• CAS No.: 2143-60-4
• Molecular Formula: C6H11O
• Molecular Weight: 99.1527
• Mol file: 2143-60-4.mol

Synonyms:

Chemical Property of Cyclohexyl, 1-hydroxy-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexyl, 1-hydroxy-

There total 4 articles about Cyclohexyl, 1-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanol (108-93-0) → α-hydroxycyclohexyl radical (2143-60-4)

Guidance literature:

With di-tert-butyl peroxide; In various solvent(s); Irradiation;

Reference yield:

1-hydroxycyclohexyl phenyl ketone (947-19-3) → α-hydroxycyclohexyl radical (2143-60-4) + benzoyl radical (2652-65-5)

Guidance literature:

In acetonitrile; UV-irradiation;

DOI:10.1021/ja026099m

Reference yield:

cyclohexanol (108-93-0) → α-hydroxycyclohexyl radical (2143-60-4) + cyclohexyloxy radical (3384-35-8) + hexanoyl (74705-65-0) + 6-oxohexyl radical (59282-49-4) + C6H11O (120158-78-3)

Guidance literature:

With lead(IV) acetate; copper(II) sulfate; In benzene; at 80 ℃; for 3.5h; Mechanism; the formation of radical products was proven by ESR spectra in the presence of spin traps;

DOI:10.1007/BF00953412

upstream raw materials:

cyclohexanol

1-hydroxycyclohexyl phenyl ketone

Refernces

• 1、 Hunt, Paula,Worrall, David R.,Wilkinson, Frank,Batchelor, Stephen N.. "Quantitative rate constants for radical reactions in the nanopores of cotton". . p. 8532 - 8533. Retrieved 2002.
• 2、 Colley, Christopher S.,Grills, David C.,Besley, Nicholas A.,Jockusch, Steffen,Matousek, Pavel,Parker, Anthony W.,Towrie, Michael,Turro, Nicholas J.,Gill, Peter M. W.,George, Michael W.. "Probing the reactivity of photoinitiators for free radical polymerization: Time-resolved infrared spectroscopic study of benzoyl radicals". . p. 14952 - 14958. Retrieved 2007/10/03.