Benzene, hexamethoxy-

Base Information

• Chemical Name: Benzene, hexamethoxy-
• CAS No.: 22015-34-5
• Molecular Formula: C12H18O6
• Molecular Weight: 258.26800
• DSSTox Substance ID: DTXSID90365332
• Nikkaji Number: J1.759.269F
• Wikidata: Q82149919
• Mol file: 22015-34-5.mol

Synonyms:Benzene, hexamethoxy-;1,2,3,4,5,6-hexamethoxybenzene;22015-34-5;hexamethoxybenzene;SCHEMBL8213378;DTXSID90365332

Chemical Property of Benzene, hexamethoxy-

Chemical Property:

• PSA: 55.38000
• LogP: 1.73820
• XLogP3: 1.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 6
• Exact Mass: 258.11033829
• Heavy Atom Count: 18
• Complexity: 163

Purity/Quality:

1,2,3,4,5,6-HEXAMETHOXYBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C(=C(C(=C1OC)OC)OC)OC)OC

Technology Process of Benzene, hexamethoxy-

There total 6 articles about Benzene, hexamethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + benzenehexol (608-80-0) → hexamethoxy-benzene (22015-34-5)

Guidance literature:

With methanol;

DOI:10.1021/ja01189a030

Reference yield:

→ hexamethoxy-benzene (22015-34-5)

Guidance literature:

With hydrogenchloride; anschliessendes Erhitzen mit wss. NaOH und Dimethylsulfat bis auf Siedetemperatur;

DOI:10.1039/jr9410000660

Reference yield:

2-hydroxy-3,4,5,6-tetramethoxyacetophenone (3162-28-5) → hexamethoxy-benzene (22015-34-5)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; Erwaermen des in wss. Aceton geloesten Reaktionsprodukts mit wss. KOH und Dimethylsulfat;

DOI:10.1039/jr9410000662

upstream raw materials:

diazomethane

benzenehexol

2,3,5,6-tetramethoxy-hydroquinone

2-hydroxy-3,4,5,6-tetramethoxyacetophenone

Downstream raw materials:

2,2-Dihydroxy-4,5,6,6-tetramethoxy-cyclohex-4-ene-1,3-dione