(4aS)-1,2,3,4,4aα,5,6,7,8,8aβ,9,9aβ,10,10aα-Tetradecahydroanthracene

Base Information

• Chemical Name: (4aS)-1,2,3,4,4aα,5,6,7,8,8aβ,9,9aβ,10,10aα-Tetradecahydroanthracene
• CAS No.: 1755-19-7
• Molecular Formula: C14H24
• Molecular Weight: 192.345
• Mol file: 1755-19-7.mol

Synonyms:Anthracene,1,2,3,4,4aa,5,6,7,8,8ab,9,9ab,10,10aa-tetradecahydro- (8CI); Anthracene, tetradecahydro-, (4aa,8ab,9ab,10aa)-;trans-syn-trans-Perhydroanthracene; trans-syn-trans-Tetradecahydroanthracene

Chemical Property of (4aS)-1,2,3,4,4aα,5,6,7,8,8aβ,9,9aβ,10,10aα-Tetradecahydroanthracene

Chemical Property:

• Refractive Index: 1.5600 (estimate)
• Boiling Point: 263.35°C (rough estimate)
• PSA: 0.00000
• Density: 0.9200 (rough estimate)
• LogP: 4.39300

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4aS)-1,2,3,4,4aα,5,6,7,8,8aβ,9,9aβ,10,10aα-Tetradecahydroanthracene

There total 40 articles about (4aS)-1,2,3,4,4aα,5,6,7,8,8aβ,9,9aβ,10,10aα-Tetradecahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

anthracene (120-12-7) → (4aR,8aS,9aR,10aS)-tetradecahydroanthracene (1755-19-7)

Guidance literature:

With hydrogenchloride; zinc; at 20 ℃; for 6h;

DOI:10.1039/a901302d

Reference yield: 25.0%

anthracene (120-12-7) → 9,10-dihydroanthracene (613-31-0) + (4aR,8aS,9aR,10aS)-tetradecahydroanthracene (1755-19-7) + (4aRS,9aRS)-1,2,3,4,4a,9,9a,10-octahydroanthracene (77341-12-9)

Guidance literature:

With hydrogenchloride; aluminium trichloride; 1-butyl-3-methylimidazolium chloride; aluminium; at 20 ℃; for 24h;

DOI:10.1039/a901302d

Reference yield:

1,2,3,4,5,6,7,8-octahydroanthracene (1079-71-6) → (4aR,8aS,9aR,10aS)-tetradecahydroanthracene (1755-19-7)

Guidance literature:

With cyclohexane; nickel; at 200 ℃; under 84583.4 - 110326 Torr; Hydrogenation;

DOI:10.1039/jr9440000286

upstream raw materials:

tetralin

anthracene

1,2,3,4,5,6,7,8-octahydroanthracene

(4aR,8aS,9aS,10aR)-tetradecahydroanthracene

Downstream raw materials:

anthracene

dihydrophenanthrene

Refernces

• 1、 Hill,R.K. et al.. "-". . p. 4006 - 4013. Retrieved 1961.
• 2、 Clarke. "". . p. 965. Retrieved 1961.
• 3、 Qi, Shi-Chao,Zhang, Lu,Wei, Xian-Yong,Hayashi, Jun-Ichiro,Zong, Zhi-Min,Guo, Lu-Lu. "Deep hydrogenation of coal tar over a Ni/ZSM-5 catalyst". . p. 17105 - 17109. Retrieved 2014/05/06.