Borinic acid, dihexyl-, methyl ester

Base Information Edit

Chemical Name:Borinic acid, dihexyl-, methyl ester
CAS No.:2344-22-1
Molecular Formula:C13H29BO
Molecular Weight:212.184
Hs Code.:
Mol file:2344-22-1.mol

Synonyms:

Suppliers and Price of Borinic acid, dihexyl-, methyl ester

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Borinic acid, dihexyl-, methyl ester Edit

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Borinic acid, dihexyl-, methyl ester

There total 1 articles about Borinic acid, dihexyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 148163-04-6
(2,4,6-triisopropylphenyl)dihexylborane

: 2344-22-1
methyl dihexylborinic ester

: 21524-34-5
2,4,6-triisopropyl-1-bromobenzene

Guidance literature:: With methanol; water; bromine; Bromination of starting compd.;

Reference yield:

: 2344-22-1
methyl dihexylborinic ester

: 614-54-0
1-phenylheptan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran; diethyl ether / 3 h / 20 °C

2.1: LHMDS / tetrahydrofuran / 2 h / -78 °C

2.2: tetrahydrofuran / -110 - 0 °C

2.3: 63 percent / aq. NaOH; H₂O₂ / tetrahydrofuran / 8 h / 20 °C

With lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether;
DOI:10.1039/b514987h