2-Bromopropanoic acid octyl ester

Base Information

• Chemical Name: 2-Bromopropanoic acid octyl ester
• CAS No.: 24625-82-9
• Molecular Formula: C11H21BrO2
• Molecular Weight: 265.191
• Mol file: 24625-82-9.mol

Synonyms:Propanoic acid,2-bromo-,octyl ester;DL-Octyl-(2-brom-propionat);DL-octyl-(2-bromo propionate);2-Bromopropionic acid,octyl ester;

Chemical Property of 2-Bromopropanoic acid octyl ester

Chemical Property:

• PSA: 26.30000
• LogP: 3.67350

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Bromopropanoic acid octyl ester

There total 2 articles about 2-Bromopropanoic acid octyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.1%

octanol (111-87-5) + Methyl 2-bromopropionate (5445-17-0) → Octyl α-bromopropionate (24625-82-9)

Guidance literature:

With titanium(IV) isopropylate; In octane; at 80 ℃; for 9.5h; Dean-Stark; Reflux;

DOI:10.1002/jhet.2026

Reference yield:

octanol (111-87-5) + 2-Bromopropionic acid (598-72-1,10327-08-9) + 2-Bromopropionyl chloride (7148-74-5) → Octyl α-bromopropionate (24625-82-9)

Guidance literature:

DOI:10.1021/jo01164a001

Reference yield: 96.1%

4-(4,6-di([1,1’-biphenyl]-4-yl)-1,3,5-triazin-2-yl)benzene-1,3-diol + Octyl α-bromopropionate (24625-82-9) → 2-(2-hydroxy-4-{1-octyloxycarbonylethyloxy}-phenyl)-4,6-bis-(4-biphenylyl)-1,3,5-triazine

Guidance literature:

2,4-bis(biphenyl-4-yl)-6-((2,4-dihydroxy)phenyl)-1,3,5-triazine; With potassium carbonate; In acetone; at 40 ℃; for 0.5h;

Octyl α-bromopropionate; In acetone; for 6h; Reflux;

DOI:10.1002/jhet.2026

upstream raw materials:

octanol

2-Bromopropionic acid

2-Bromopropionyl chloride

Methyl 2-bromopropionate

Downstream raw materials:

octyl propionate

Refernces