1,12-Diiodododecane

Base Information

• Chemical Name: 1,12-Diiodododecane
• CAS No.: 24772-65-4
• Molecular Formula: C12H24I2
• Molecular Weight: 422.132
• DSSTox Substance ID: DTXSID30462859
• Nikkaji Number: J1.467.935I
• Wikidata: Q82287475
• Mol file: 24772-65-4.mol

Synonyms:1,12-diiodododecane;Dodecane, 1,12-diiodo-;24772-65-4;SCHEMBL3642089;DTXSID30462859;BRNHWOARSGSQED-UHFFFAOYSA-N

Chemical Property of 1,12-Diiodododecane

Chemical Property:

• Refractive Index: 1.4747 (estimate)
• Boiling Point: 363.34°C (estimate)
• PSA: 0.00000
• Density: 1.6185 (rough estimate)
• LogP: 5.75740
• XLogP3: 7.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 11
• Exact Mass: 421.99675
• Heavy Atom Count: 14
• Complexity: 82.3

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C(CCCCCCI)CCCCCI

Technology Process of 1,12-Diiodododecane

There total 14 articles about 1,12-Diiodododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,12-dibromododecane (3344-70-5) → 1,12-diiodododecane (24772-65-4)

Guidance literature:

With sodium iodide; In acetone; for 24h; Inert atmosphere; Reflux;

DOI:10.1039/c2ob06859a

Reference yield: 70.0%

dodecane-1,12-diyl bis(4-methylbenzenesulfonate) (36247-34-4) → 1,12-diiodododecane (24772-65-4)

Guidance literature:

With sodium iodide; In acetone; for 12h; Reflux;

Reference yield:

1,12-dodecandiol (5675-51-4) → 1,12-diiodododecane (24772-65-4)

Guidance literature:

With phosphorus; iodine; at 150 ℃;

upstream raw materials:

1,12-dodecandiol

4,4'-[1,12-dodecanediylbis(oxy)]bisbenzene

1,12-bis-(2-methoxy-phenoxy)-dodecane

1,12-dibromododecane

Downstream raw materials:

1,1,1,14,14,14-Hexaphenyltetradecan

C₅₀H₅₄*C₂₉H₅₈

4,4'-(1,1'-(dodecane-1,12-diyl)bis(pyridin-1(1H)-yl-4(1H)-ylidene)bis(cyclohexa-2,5-dienone))

1,24-bis-(4-methoxy-phenoxy)-tetracosane

Refernces

• 1、 -. "BIVALENT BROMODOMAIN LIGANDS, AND METHODS OF USING SAME". . . Retrieved 2015/06/11.
• 2、 Sheibani, Esmaeil,Waernmark, Kenneth. "Conformationally restricted dynamic supramolecular catalysts for substrate-selective epoxidations". experimental part. p. 2059 - 2067. Retrieved 2012/04/23.