Technology Process of 1-Propanone, 2-methyl-1,3-bis(4-methylphenyl)-
There total 6 articles about 1-Propanone, 2-methyl-1,3-bis(4-methylphenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / methanol; water / 1 h / 0 - 20 °C
1.2: 20 °C
2.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0 - 20 °C
3.1: trifuran-2-yl-phosphane; palladium diacetate; lithium tert-butoxide / 24 h / 130 °C / Sealed tube; Inert atmosphere
With
methanol; sodium tetrahydroborate; trifuran-2-yl-phosphane; palladium diacetate; sodium hydroxide; lithium tert-butoxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1002/adsc.202101101
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / methanol; water / 1 h / 0 - 20 °C
1.2: 20 °C
2.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0 - 20 °C
3.1: trifuran-2-yl-phosphane; palladium diacetate; lithium tert-butoxide / 24 h / 130 °C / Sealed tube; Inert atmosphere
With
methanol; sodium tetrahydroborate; trifuran-2-yl-phosphane; palladium diacetate; sodium hydroxide; lithium tert-butoxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1002/adsc.202101101