tetracarbonyl(N,N'-dicyclohexyldithiooxamide)molybdenum

Base Information

• Chemical Name: tetracarbonyl(N,N'-dicyclohexyldithiooxamide)molybdenum
• CAS No.: 93976-50-2
• Molecular Formula: C₁₈H₂₄MoN₂O₄S₂
• Molecular Weight: 492.472
• Mol file: 93976-50-2.mol

Synonyms:

Chemical Property of tetracarbonyl(N,N'-dicyclohexyldithiooxamide)molybdenum

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetracarbonyl(N,N'-dicyclohexyldithiooxamide)molybdenum

There total 1 articles about tetracarbonyl(N,N'-dicyclohexyldithiooxamide)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-tetracarbonylbis(triphenylphosphine oxide)molybdenum (60966-87-2) + N,N'-dicyclohexyldithiooxamide (122-36-1) → tetracarbonyl(N,N'-dicyclohexyldithiooxamide)molybdenum (93976-50-2)

Guidance literature:

In diethyl ether; byproducts: Ph3PO; (under N2); addn. of the oxamide to a soln. of the starting complex in ether, stirring for 36 h at room temp., cooling to 0°C; filtn. after 1 h from Ph3PO, evapn. of the soln. to dryness, dissolvingof the residue in hexane, yield 20-55 %, elem. anal.;

upstream raw materials:

cis-tetracarbonylbis(triphenylphosphine oxide)molybdenum

N,N'-dicyclohexyldithiooxamide