Oxaziridine, 2-cyclohexyl-3,3-dimethyl-

Base Information

• Chemical Name: Oxaziridine, 2-cyclohexyl-3,3-dimethyl-
• CAS No.: 2763-76-0
• Molecular Formula: C9H17NO
• Molecular Weight: 155.24
• Mol file: 2763-76-0.mol

Synonyms:

Chemical Property of Oxaziridine, 2-cyclohexyl-3,3-dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Oxaziridine, 2-cyclohexyl-3,3-dimethyl-

There total 2 articles about Oxaziridine, 2-cyclohexyl-3,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

cyclohexylamine (108-91-8,157973-60-9) + acetone (67-64-1) → 2-Cyclohexyl-3,3-dimethyloxaziridine (2763-76-0) + cyclohexanone-oxime (100-64-1) + N,N'-dicyclohexyldiazene N,N'-dioxide (3378-45-8,17606-86-9,26049-06-9) + 1-nitrocyclohexane (1122-60-7)

Guidance literature:

With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; sodium hydrogencarbonate; In dichloromethane; water;

DOI:10.1021/jo00051a017

Reference yield:

→ 2-Cyclohexyl-3,3-dimethyloxaziridine (2763-76-0)

Guidance literature:

(CH3)2C=C(CH3)2, Cyclohexylamin, in E. oder CCl4, -20gradC, Ozon;

upstream raw materials:

cyclohexylamine

acetone

Refernces

• 1、 Crandall, Jack K.,Reix, Thierry. "Dimethyldioxirane Oxidation of Primary Amines". . p. 6759 - 6764. Retrieved 2007/10/02.