9-Heptadecanol

Base Information

• Chemical Name: 9-Heptadecanol
• CAS No.: 624-08-8
• Molecular Formula: C17H36O
• Molecular Weight: 256.472
• Hs Code.: 2905199090
• Mol file: 624-08-8.mol

Synonyms:9-HEPTADECANOL;NISTC624088;Heptadecan-9-ol

Chemical Property of 9-Heptadecanol

Chemical Property:

• Vapor Pressure: 3.05E-05mmHg at 25°C
• Melting Point: 58.0 to 62.0 °C
• Refractive Index: 1.448
• Boiling Point: 318.2 °C at 760 mmHg
• PKA: 15.28±0.20(Predicted)
• Flash Point: 122 °C
• PSA: 20.23000
• Density: 0.835 g/cm³
• LogP: 5.84850
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%,99%, ^*data from raw suppliers

9-Heptadecanol >95.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-Heptadecanol

There total 17 articles about 9-Heptadecanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-bromo-octane (111-83-1) + formic acid ethyl ester (109-94-4) → 9-heptadecanol (624-08-8)

Guidance literature:

1-bromo-octane; With iodine; magnesium; In tetrahydrofuran; at 0 - 60 ℃; for 2h; Inert atmosphere;

formic acid ethyl ester; In tetrahydrofuran; at 0 - 60 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.201912556

Reference yield: 90.0%

heptadecan-9-one (540-08-9) → 9-heptadecanol (624-08-8)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 1h;

Reference yield: 90.0%

nonan-1-al (124-19-6) + n-chlorooctane (111-85-3) → 9-heptadecanol (624-08-8)

Guidance literature:

With iodine; magnesium; In diethyl ether; at 25 ℃; Inert atmosphere;

DOI:10.1002/cplu.201900593

upstream raw materials:

nonan-1-al

octylmagnesium bromide

heptadec-8-ene

heptadecan-9-one

Downstream raw materials:

9-(4-methylbenzenesulfonate)-9-heptadecanol

9-(9-heptadecanyl)-2,7-diformylcarbazole

heptadecan-9-one

heptadecan-9-yl 8-((2-hydroxyethyl)(8-(nonyloxy)-8-oxooctyl)amino)octanoate

Refernces

• 1、 -. "Long-chain alkyl ester amine compound or fluorine-containing long-chain alkyl ester amine compound and kilogram-level preparation method thereof". Paragraph 0131-0132; 0153; 0190-0191; 0193. . Retrieved 2021/09/15.
• 2、 Rao, Jiancheng,Liu, Xinrui,Li, Xuefei,Yang, Liuqing,Zhao, Lei,Wang, Shumeng,Ding, Junqiao,Wang, Lixiang. "Bridging Small Molecules to Conjugated Polymers: Efficient Thermally Activated Delayed Fluorescence with a Methyl-Substituted Phenylene Linker". supporting information. p. 1320 - 1326. Retrieved 2019/12/24.