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1001911-63-2

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Basic Information
CAS No.: 1001911-63-2
Name: (9-phenyl-9H-carbazol-2-yl)boronic acid
Article Data: 18
Molecular Structure:
Molecular Structure of 1001911-63-2 ((9-phenyl-9H-carbazol-2-yl)boronic acid)
Formula: C18 H14 BNO2
Molecular Weight: 287.126
Synonyms: (9-phenyl-9H-carbazol-2-yl)boronic acid;(9-phenyl-9H-carbazol-2-yl)boronic acid (2PCBA);9-Phenylcarbazole-2-boronic acid;B-(9-Phenyl-9H-carbazol-2-yl)-boronic acid;2-BAPC
Density: 1.20±0.1 g/cm3(Predicted)
Boiling Point: 466.0±51.0 °C(Predicted)
PSA: 45.39000
LogP: 2.46350
Related products
Synthetic route
5419-55-6

Triisopropyl borate

94994-62-4

9-(phenyl)-2-bromo-9H-carbazole

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -75 - 0℃; for 1h; Inert atmosphere;
Stage #2: Triisopropyl borate In tetrahydrofuran at -70 - 20℃; for 12h; Inert atmosphere;
Stage #3: With hydrogenchloride In tetrahydrofuran; water for 0.5h; Temperature; Inert atmosphere;		95%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran for 1h;
Stage #2: Triisopropyl borate In tetrahydrofuran at 20℃; for 12h;		78.4%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h;
Stage #2: Triisopropyl borate In diethyl ether; hexane at -78 - 20℃;
Stage #3: With hydrogenchloride In diethyl ether; hexane		78%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -78℃; for 1h;
Stage #2: Triisopropyl borate In tetrahydrofuran		70%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -78℃; for 0.666667h;
Stage #2: Triisopropyl borate In tetrahydrofuran at 20℃; for 12h;
Stage #3: With water In tetrahydrofuran; hexane		62.8%
121-43-7

Trimethyl borate

94994-62-4

9-(phenyl)-2-bromo-9H-carbazole

7732-18-5

water

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -78 - 0℃; for 1h;
Stage #2: Trimethyl borate In tetrahydrofuran at -78 - 20℃; for 12h;
Stage #3: water With hydrogenchloride In tetrahydrofuran		81%
...Expand
121-43-7

Trimethyl borate

94994-62-4

9-(phenyl)-2-bromo-9H-carbazole

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -78 - 0℃; for 1h; Inert atmosphere;
Stage #2: Trimethyl borate In tetrahydrofuran at -78 - 20℃; for 12h;		79%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -78℃; for 2h; Inert atmosphere;
Stage #2: Trimethyl borate In tetrahydrofuran at 20℃; for 4h; Inert atmosphere;		72%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h;
Stage #2: Trimethyl borate In tetrahydrofuran; hexane for 12h;
Stage #3: With water		69%
With n-butyllithium
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium at -78℃;
Stage #2: Trimethyl borate at -78℃;
Stage #3: With hydrogenchloride In water
7647-01-0

hydrogenchloride

121-43-7

Trimethyl borate

94994-62-4

9-(phenyl)-2-bromo-9H-carbazole

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Stage #1: Trimethyl borate; 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran at -78 - 20℃;
Stage #2: hydrogenchloride In tetrahydrofuran		76%
...Expand
94994-62-4

9-(phenyl)-2-bromo-9H-carbazole

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h;
Stage #2: With Trimethyl borate In tetrahydrofuran; hexane at 20℃; for 12h;
Stage #3: With water In tetrahydrofuran; hexane		69%
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h;
Stage #2: With Triisopropyl borate In tetrahydrofuran; hexane at -78 - 20℃; for 12h;
Stage #3: With water In tetrahydrofuran; hexane at 20℃;		67.33%
With hydrogenchloride; n-butyllithium; Trimethyl borate In water Inert atmosphere;
5419-55-6

Triisopropyl borate

94994-62-4

9-(phenyl)-2-bromo-9H-carbazole

7732-18-5

water

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Stage #1: 9-(phenyl)-2-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran; hexane for 0.5h;
Stage #2: Triisopropyl borate In tetrahydrofuran; hexane at 20℃; for 5h;
Stage #3: water With hydrogenchloride In tetrahydrofuran; hexane; water for 0.5h;		55%
...Expand
5467-74-3

4-Bromophenylboronic acid

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene / 4 h / 100 °C
2.1: triethyl phosphite / 6 h / 150 °C
3.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
3.2: 14 h / Reflux
4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
4.2: 12 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene / 4 h / 100 °C
2.1: triethyl phosphite / 6 h / 150 °C
3.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
3.2: 14 h / Reflux
4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
4.2: 12 h
View Scheme
35450-34-1

4'-bromo-2-nitrobiphenyl

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: triethyl phosphite / 6 h / 150 °C
2.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
2.2: 14 h / Reflux
3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
3.2: 12 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: triethyl phosphite / 6 h / 150 °C
2.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
2.2: 14 h / Reflux
3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
3.2: 12 h
View Scheme
Multi-step reaction with 3 steps
1.1: triethyl phosphate / 7 h / 150 °C
2.1: potassium phosphate; ethylenediamine / 12 h / Reflux
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
3.2: 12 h / -78 - 20 °C
3.3: 20 °C
View Scheme
3652-90-2

2-bromo-9H-carbazole

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
1.2: 14 h / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
2.2: 12 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
1.2: 14 h / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
2.2: 12 h
View Scheme
Multi-step reaction with 2 steps
1.1: caesium carbonate; copper(l) iodide; ethylenediamine / toluene / 12 h / Reflux
2.1: n-butyllithium / tetrahydrofuran / 1 h
2.2: 12 h / 20 °C
View Scheme
609-73-4

o-nitroiodobenzene

1001911-63-2

(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene / 4 h / 100 °C
2.1: triethyl phosphite / 6 h / 150 °C
3.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
3.2: 14 h / Reflux
4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
4.2: 12 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene / 4 h / 100 °C
2.1: triethyl phosphite / 6 h / 150 °C
3.1: caesium carbonate / copper(l) iodide / toluene / 50 °C
3.2: 14 h / Reflux
4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C
4.2: 12 h
View Scheme
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    1001911-63-2

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    1001911-63-2

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    ProName: (9-phenyl-9H-carbazol-2-yl)boronic aci... CasNo: 1001911-63-2 Molecular Formula: C18H14BNO2 Appearance: solid Application: auxiliaries DeliveryTime: 20day PackAge: meet customer's demand Port: shanghai ProductionCapacity: 5 Met

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    1001911-63-2

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    1001911-63-2

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    1001911-63-2

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    1001911-63-2

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  • Casno:

    1001911-63-2

    1001911-63-2 (9-phenyl-9H-carbazol-2-yl)boronic acid CAS NO.1001911-63-2

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    1001911-63-2

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    1001911-63-2

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    Product name: N-Phenyl-9H-Carbazole-2-Boronic Acid CAS No.：1001911-63-2 Molecule Formula：C18H14BNO2 Molecule Weight：287.12 Purity: 99.0% Package: 25kg/drum Description：White crystalline powder Manufacture Standards：Enterprise Standard

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    1001911-63-2

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    1001911-63-2

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    1001911-63-2

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    1001911-63-2

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    1001911-63-2

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    Min.Order: 1 Gram

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  • Casno:

    1001911-63-2

    (9-phenyl-9H-carbazol-2-yl)boronic acid

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  • 1001911-63-2 CAS NO.1001911-63-2

  • Casno:

    1001911-63-2

    1001911-63-2 CAS NO.1001911-63-2

    Min.Order: 1 Metric Ton

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