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109-63-7

Basic Information
CAS No.: 109-63-7
Name: Boron trifluoride etherate
Article Data: 31
Molecular Structure:
Molecular Structure of 109-63-7 (Boron trifluoride etherate)
Formula: C4H10BF3O
Molecular Weight: 141.929
Synonyms: (Diethylether)trifluoroboron;Boron fluoride diethyl ether complex;Boron fluoridediethyl etherate;Boron fluoride etherate;Boron fluoride monoetherate;Boronfluoride-diethyl ether compound;Boron fluoride-ethyl ether complex;Boronfluoride-ethyl etherate;Boron trifluoride etherate(1:1);Boron trifluoride ethyl etherate (1:1);Boron trifluoride monoetherate;Boron trifluoride-diethyl ether (1:1);Boron trifluoride-diethyl ether 1:1complex;Boron trifluoride-diethyl ether complex;Boron trifluoride-diethylether complex (1:1);Trifluoroborane diethyl etherate;Trifluoro[1,1'-oxybis[ethane]]boron;Trifluoro(diethyl ether)boron;Ethylether-boron trifluoride complex;Boron trifluoride-diethyl etherate;Borontrifluoride-ether complex;Boron trifluoride-ethyl ether;Borontrifluoride-ethyl ether (1:1);Boron trifluoride-ethyl ether complex;Borontrifluoride-ethyl etherate;Diethyl ether compound with boron trifluoride;Diethylether trifluoroborane complex;Diethyl ether-trifluoroborane (1:1);Trifluoroboron etherate;Trifluoroborane-1,1'-oxybis[ethane] (1:1);Trifluoroboron-diethyl ether (1:1);(Diethyl ether)trifluoroborane;
EINECS: 203-689-8
Density: 1.12 g/cm3
Melting Point: -58 °C(lit.)
Boiling Point: 126 dec
Flash Point: 118°F
Solubility: Reacts with water
Appearance: colourless to brown fuming liquid with anacrid odour
Hazard Symbols: ToxicT,CorrosiveC
Risk Codes: 10-14-20/22-35-48/23-34-14/15
Safety: 16-23-26-36/37/39-45-8-28A-43
Transport Information: UN 2604 8/PG 1
PSA: 17.07000
LogP: 1.92260
Synthetic route
444-40-6

2,4,6-tris(trilfuoromethyl)phenyllithium

10294-34-5

boron trichloride

A

99919-68-3

BF2Cl*Et2O

B

99919-69-4

BFCl2*Et2O

C

109-63-7

boron trifluoride diethyl etherate

D

681812-01-1

2,4,6-(CF3)3C6H2BCl2

E

681812-02-2

bis-(2,4,6-tris-trifluoromethyl-phenyl) fluoroborane

Conditions
ConditionsYield
In diethyl ether under an inert atm.; to a soln. of Li-contg. compd. in hexanes and Et2O was added dropwise an excess of B-contg. compd. (1 M in heptane) at -78°C ; the react. mixt. was allowed to warm to room temp. for 6 h; the soln. was filtered and the solvents were removed under vac.; a mixt.of yellow oil and white solid; the mixt. was vac. distd. at 60°C /0.05 Torr; the residue was sublimed at 95°C under vac.;A n/a
B n/a
C n/a
D 5%
E 24%
109-63-7

boron trifluoride diethyl etherate

99179-72-3

3-acetoxy-4-methoxyphenol

7298-21-7

1-(2,4-dihydroxy-5-methoxyphenyl)ethan-1-one

Conditions
ConditionsYield
at 70℃; for 2h;100%
109-63-7

boron trifluoride diethyl etherate

675837-54-4

1-[bis(diisopropylamino)boryl]imidazole

675837-55-5

1-[bis(diisopropylamino)boryl]imidazole(N(3)-B)trifuoroborane

Conditions
ConditionsYield
In tetrahydrofuran under Ar; BF3*OEt2 added to soln. of N-compd. in THF at -78°C, mixt. allowed to warm to room temp., stirred for 7 h; evapn. of solvent;100%
109-63-7

boron trifluoride diethyl etherate

123-54-6

acetylacetone

15390-25-7

(acetylacetonato)borondifluoride

Conditions
ConditionsYield
With potassium carbonate In dichloromethane at 20℃; for 0.5h;100%
In dichloromethane for 12h; Inert atmosphere;96%
With diphenyl acetylene In dichloromethane at 20℃; for 12h;83%
946613-44-1

C2H5OCOC4N(CH3)2CHC4H2N(OCH3)C4H4N*HCl

109-63-7

boron trifluoride diethyl etherate

1318245-52-1

[(C2H5OCOC4N(CH3)2CHC4HN(OCH3)C4H3NH)BF2]

Conditions
ConditionsYield
With (C2H5)3N In dichloromethane (C2H5)3N added to a soln. of ligand salt under N2, stirred for 10 min, Bcomplex added, stirred at room temp. for 2 h; poured into an aq. soln. of citric acid, extd. (ether), the org. layer washed with aq. citric acid, dried (Na2SO4), concd. (vac.), filtered (silica, CH2Cl2), concd. (vac.);100%
109-63-7

boron trifluoride diethyl etherate

1430883-93-4

(1E,4Z,6E)-5-hydroxy-4-(3-methoxyphenyl)-1,7-bis(4-methoxyphenyl)hepta-1,4,6-trien-3-one

(1E,4Z,6E)-5-(difluoroboryloxy)-4-(3-methoxyphenyl)-1,7-bis(4-methoxyphenyl)hepta-1,4,6-trien-3-one

Conditions
ConditionsYield
In dichloromethane Reflux;100%
109-63-7

boron trifluoride diethyl etherate

1430883-95-6

(1E,4Z,6E)-5-hydroxy-1,4,7-tris(4-methoxyphenyl)hepta-1,4,6-trien-3-one

(1E,4Z,6E)-5-(difluoroboryloxy)-1,4,7-tris(4-methoxyphenyl)hepta-1,4,6-trien-3-one

Conditions
ConditionsYield
In dichloromethane Reflux;100%
109-63-7

boron trifluoride diethyl etherate

1430883-98-9

methyl 4-((1E,3Z,6E)-3-hydroxy-1,7-bis(4-methoxyphenyl)-5-oxohepta-1,3,6-trien-4-yl)benzoate

(1E,4Z,6E)-5-(difluoroboryloxy)-4-(4-methoxyphenyl)-1,7-bis(4-methoxyphenyl)hepta-1,4,6-trien-3-one

Conditions
ConditionsYield
In dichloromethane Reflux;100%
109-63-7

boron trifluoride diethyl etherate

1430884-00-6

(1E,4Z,6E)-5-hydroxy-1,7-bis(4-methoxyphenyl)-4-phenylhepta-1,4,6-trien-3-one

(1E,4Z,6E)-5-(difluoroboryloxy)-1,7-bis(4-methoxyphenyl)-4-phenylhepta-1,4,6-trien-3-one

Conditions
ConditionsYield
In dichloromethane Reflux;100%
109-63-7

boron trifluoride diethyl etherate

1430884-04-0

(1E,4Z,6E)-5-hydroxy-1,7-bis(4-methoxynaphthalen-1-yl)-4-phenylhepta-1,4,6-trien-3-one

(1E,4Z,6E)-5-(difluoroboryloxy)-1,7-bis(4-methoxynaphthalen-1-yl)-4-phenylhepta-1,4,6-trien-3-one

Conditions
ConditionsYield
In dichloromethane Reflux;100%
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    Product name: Boron Trifluoride Diethyl Etherate CAS No.: 109-63-7 Molecule Formula:C4H10BF3O Molecule Weight:141.93 Purity: 46.8% Package: 200kg/drum Description:Colorless or yellowish transparent liquid Manufacture Standards:Enterpr

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  • Boron trifluoride etherate CAS NO.109-63-7  CAS NO.109-63-7

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Chemistry

Product Name:Boron trifluoride etherate(109-63-7)
CAS No:109-63-7
MF: C4H10BF3O
MW: 141.93
mp : -58 °C(lit.)
bp : 126-129 °C(lit.)
density : 1.15 g/mL(lit.)
vapor density : 4.9 (vs air)
vapor pressure : 4.2 mm Hg ( 20 °C)
refractive index : n20/D 1.344(lit.)
Fp : 118 °F
storage temp. : 2-8°C
form : liquid
color : brown
Water Solubility : Reacts
Sensitive : Moisture Sensitive
Synonyms of Boron trifluoride etherate(109-63-7): 1'-oxybis[ethane]]-trifluoro[(beta-4)-boro;bf3-ethercomplex;Borane, trifluoro-, compd. with 1,1'-oxybis(ethane) (1:1);borane,trifluoro-,cmpdwith1,1'-oxybis(ethane)(1:1);Borane,trifluoro-,compd.with1,1'-oxybis[ethane](1:1);Boron fluoride diethyl etherate;Boron fluoride etherate;Boron fluoride monoetherate
Molecular Structure of Boron trifluoride etherate(109-63-7):

Boron trifluoride etherate(109-63-7) is a fuming liquid. Boron trifluoride etherate may be corrosive to skin, eyes and mucous membranes. Boron trifluoride etherate(109-63-7) may be toxic by inhalation. Upon exposure to water Boron trifluoride etherate may emit flammable and corrosive vapors. Boron trifluoride etherate is used as a catalyst in chemical reactions.

Toxicity Data With Reference

RTECS#: CAS# 109-63-7: None listed
LD50/LC50: RTECS: Not available. Other: Oral, rat: LD50 = 496 mg/kg 
Carcinogenicity: Boron trifluoride etherate - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: The toxicological properties have not been fully investigated.

Safety Profile

Hazard Codes : T,C
Risk Statements : 10-14-20/22-35-48/23-34-14/15
Safety Statements : 16-23-26-36/37/39-45-8-28A-43
RIDADR : UN 2604 8/PG 1
WGK Germany : 3
F : 10 
HazardClass : 8
PackingGroup : I

Specification

Boron trifluoride etherate(109-63-7)`s Categories: Industrial/Fine Chemicals;Organometallics;Boron Trifluorides;Boron Trihalides;B (Classes of Boron Compounds);Biochemistry;Reagents for Oligosaccharide Synthesis;Fluoro series

Handling: Do not allow water to get into the container because of violent reaction. Do not breathe dust, vapor, mist, or gas. Do not get in eyes, on skin, or on clothing. Take precautionary measures against static discharges. Do not ingest or inhale. Use and store under nitrogen. Use only in a chemical fume hood. This product may be under pressure; cool before opening. 
Storage: Keep away from heat and flame. Store in a cool, dry place. Store in a tightly closed container. Flammables-area. Store protected from moisture. Store under an inert atmosphere.