CAS No.110-26-9,N,N'-Methylenebisacrylamide Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	110-26-9
Name:	N,N'-Methylenebisacrylamide

Formula:	C₇H₁₀N₂O₂
Molecular Weight:	154.169
Synonyms:	Acrylamide,N,N'-methylenebis- (6CI,7CI,8CI);Bisacrylamide;Methylenebisacrylamide;Methylenediacrylamide;N,N'-Diacryloylmethylenediamine;N,N'-Methylenebis(2-propenamide);N,N'-Methylenebis(acrylamide);2-Propenamide,N,N'-methylenebis-;NSC 406836;NSC 7774;Triam 507;
EINECS:	203-750-9
Density:	1.054 g/cm³
Melting Point:	>300 °C(lit.)
Boiling Point:	445.1 °C at 760 mmHg
Flash Point:	215 °C
Solubility:	0.01-0.1 g/100 mL at 18 °C in water
Appearance:	white crystalline powder
Hazard Symbols:	Xn,Xi
Risk Codes:	20/22-20/21/22-36/37/38
Safety:	22-36/37-36-26
Transport Information:	UN 2811
PSA:	58.20000
LogP:	0.33010

Synthetic route

: 50-00-0
formaldehyd

: 79-06-1
2-propenamide

: 110-26-9
N,N'-Methylenebisacrylamide

Conditions

Conditions	Yield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone In water at 65 - 75℃; for 2.5h; Reagent/catalyst; Temperature;	87.54%

: 924-42-5
N-Methylolacrylamid

: 107-06-2
1,2-dichloro-ethane

: 110-26-9
N,N'-Methylenebisacrylamide

Conditions

Conditions	Yield
With hydrogenchloride

: 50-00-0
formaldehyd

: 107-06-2
1,2-dichloro-ethane

: 79-06-1
2-propenamide

: 110-26-9
N,N'-Methylenebisacrylamide

Conditions

Conditions	Yield
With hydrogenchloride

...Expand

: 50-00-0
formaldehyd

: 107-13-1
acrylonitrile

: 110-26-9
N,N'-Methylenebisacrylamide

Conditions

Conditions	Yield
With sulfuric acid; water
With hydroquinone
With sulfuric acid

: 50-00-0
formaldehyd

: 7664-93-9
sulfuric acid

: 107-13-1
acrylonitrile

: 110-26-9
N,N'-Methylenebisacrylamide

...Expand

: 115-77-5
Pentaerythritol

: 924-42-5
N-Methylolacrylamid

A: etherbis-N-methylenacrylamide

B: 85030-50-8
C13H22N2O6

C: C14H27NO8

D: C17H27N3O7

E: C26H42N4O11

F: C30H47N5O12

G: C34H52N6O13

H: C26H42N4O11

I: 110-26-9
N,N'-Methylenebisacrylamide

Conditions

Conditions	Yield
Stage #1: Pentaerythritol; N-Methylolacrylamid With tempol; toluene-4-sulfonic acid In methanol at 86℃; for 1.5h; Stage #2: With ammonia In methanol; propyleneglycol monomethylether; water

...Expand

p-(1,4,7,10,13-Pentaoxatetradecyl)benzylacetal-bisacrylamide: p-(1,4,7,10,13-Pentaoxatetradecyl)benzylacetal-bisacrylamide

: 814-68-6
acryloyl chloride

: 110-26-9
N,N'-Methylenebisacrylamide

Conditions

Conditions	Yield
With sodium hydroxide; potassium carbonate; triethylamine In 1,4-dioxane; methanol; water; ethyl acetate	200 mg (58%)

: 57-55-6
propylene glycol

: 4731-53-7
TOP

: 110-26-9
N,N'-Methylenebisacrylamide

: 110-26-9
N,N'-Methylenebisacrylamide

: 139031-06-4
bis(mesityleneformyl)phosphine

: 1591653-06-3
N,N-methylene(bis(bis(2,4,6-trimethylbenzoyl)phosphino)propanamide)

Conditions

Conditions	Yield
With triethylamine In 1,2-dimethoxyethane; toluene at 50℃; for 12h; Schlenk technique; Inert atmosphere;	99%

: 347371-56-6
N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetra[4-(2-aminoethyl)phenoxy]perylene-3,4,9,10-tetracarboxylic acid diimide

: 110-26-9
N,N'-Methylenebisacrylamide

: 1549684-13-0
C136H158N22O24

Conditions

Conditions	Yield
In methanol; water at 50℃; for 48h; Michael Addition; Inert atmosphere;	95%

Raw Materials

924-42-5

4731-53-7

50-00-0

107-06-2

57-55-6

79-06-1

7664-93-9

107-13-1

Downstream Products

79-10-7

Total:197 Page 1 of 6 1 2 3 4 5 6 Next>>

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Chemistry

Molecular structure of N,N'-Methylenebisacrylamide (CAS NO.110-26-9):

IUPAC Name: N-[(Prop-2-enoylamino)methyl]prop-2-enamide
Molecular Formula: C₇H₁₀N₂O₂
Molecular Weight: 154.1665 g/mol
Density: 1.054 g/cm³
Melting Point: >300 °C(lit.)
Boiling Point: 445.1 °C at 760 mmHg
Flash Point: 215 °C
Index of Refraction: 1.475
Molar Refractivity: 41.17 cm³
Molar Volume: 146.1 cm³
Surface Tension: 34.7 dyne/cm
Enthalpy of Vaporization: 70.3 kJ/mol
Vapour Pressure: 4.06E-08 mmHg at 25 °C
Storage Temp.: 2-8 °C
Water Solubility: 0.01-0.1 g/100 mL at 18 °C
XLogP3-AA: 0.1
H-Bond Donor: 2
H-Bond Acceptor: 2
Rotatable Bond Count: 4
Tautomer Count: 3
Exact Mass: 154.074228
MonoIsotopic Mass: 154.074228
Topological Polar Surface Area: 58.2
Heavy Atom Count: 11
Canonical SMILES: C=CC(=O)NCNC(=O)C=C
InChI: InChI=1S/C7H10N2O2/c1-3-6(10)8-5-9-7(11)4-2/h3-4H,1-2,5H2,(H,8,10)(H,9,11)
InChIKey: ZIUHHBKFKCYYJD-UHFFFAOYSA-N
EINECS: 203-750-9
Product Categories: Biochemistry; Reagents for Electrophoresis; Acrylamide; Molecular Biology; Nucleic Acid Electrophoresis

Uses

N,N'-Methylenebisacrylamide (CAS NO.110-26-9) is an important material for the separation of Amino Acids. It is essential to photosensitive nylon and plastics. N,N'-Methylenebisacrylamide is also used as plugging agent in oilfield drilling and construction grouting. It is used as cross-linking agent in the synthesis of acrylic resin and adhesives.

Toxicity Data With Reference

1.	mma-sat 1 mg/plate	EMMUEG Environmental and Molecular Mutagenesis. 11 (Suppl 12)(1988),1.
2.	dlt-mus-ipr 225 mg/kg	MUREAV Mutation Research. 229 (1990),161.
3.	orl-rat LD50:390 mg/kg	37ASAA Kirk-Othmer Encyclopedia of Chemical Technology. 1 (1978),306.
4.	orl-mus LD50:380 mg/kg	JACTDZ Journal of the American College of Toxicology. 1 (1990),111.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by ingestion. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of NO_x. See also AMIDES.
Hazard Codes: Xn, Irritant Xi
Risk Statements: 20/22-20/21/22-36/37/38
20/22: Harmful by inhalation and if swallowed
20/21/22: Harmful by inhalation, in contact with skin and if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 22-36/37-36-26
22: Do not breathe dust
36/37: Wear suitable protective clothing and gloves
36: Wear suitable protective clothing
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
RIDADR: UN 2811
WGK Germany: 2
RTECS: AS3678000
F: 8
F8: Photosensitive
HazardClass: 6.1(b)
PackingGroup: III
HS Code: 29241900

Specification

N,N'-Methylenebisacrylamide (CAS NO.110-26-9) is also named as 2-Propenamide, N,N'-methylenebis- ; 4-02-00-01472 (Beilstein Handbook Reference) ; AI3-08643 ; BRN 1706297 ; CCRIS 4672 ; Methylenebisacrylamide ; Methylenediacrylamide ; N,N'-Methylenebis(2-propenamide) ; N,N'-Methylenebis(acrylamide) ; N,N'-Methylenediacrylamide ; N,N'-Methylidenebisacrylamide ; NSC 406836 . N,N'-Methylenebisacrylamide (CAS NO.110-26-9) is white crystalline powder with a neutral odor. It is very slightly water soluble. N,N'-Methylenebisacrylamide is incompatible with strong oxidizers, strong acids and strong bases. Flash point data for N,N'-Methylenebisacrylamide are not available; however, it is probably combustible.