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33665-90-6

Basic Information
CAS No.: 33665-90-6
Name: Acesulfame
Article Data: 23
Molecular Structure:
Molecular Structure of 33665-90-6 (Acesulfame)
Formula: C4H5NO4S
Molecular Weight: 163.154
Synonyms: 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one2,2-dioxide;6-Methyl-3,4-dihydro-1,2,3-oxathiazin-4-one 2,2-dioxide;Acesulfam;Acesulfam H;Acetosulfam;
EINECS: 251-622-6
Density: 1.512 g/cm3
Melting Point: 123-123.5°
Solubility: 270 g/L at 20 °C in water
PSA: 80.85000
LogP: 0.69100
Synthetic route

6-methyl-2,3-dihydro-1,3-oxazin-2,4-dione-3-sulfo-fluoride

33665-90-6

acetosulfam

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; acetone86%
With triethylamine In water; ethyl acetate81%
With sodium hydroxide81%
With potassium hydroxide In dichloromethane; water
99911-48-5

Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure

33665-90-6

acetosulfam

Conditions
ConditionsYield
Stage #1: Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure With disulfuric acid In dichloromethane at -30 - 4℃; for 0.00116667 - 0.00569444h;
Stage #2: With water In dichloromethane at 0 - 35℃; Product distribution / selectivity;
37 - 91 %Chromat.
Stage #1: Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure With sulfur trioxide In dichloromethane at -30 - -10℃;
Stage #2: With sulfuric acid; water In dichloromethane at 15 - 25℃; Product distribution / selectivity;
70 %Chromat.
Stage #1: Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure With sulfur trioxide In dichloromethane at -35 - -25℃;
Stage #2: With water at -22 - -5℃; for 0.166667h;
Stage #1: Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure With sulfur trioxide In dichloromethane for 1.38889E-05h; Flow reactor;
Stage #2: With water Time;
85 %Chromat.
Stage #1: Triethylammoniumsalz der Acetoacetamid-N-sulfonsaeure With sulfur trioxide In dichloromethane
Stage #2: With water
5977-14-0

acetoacetamido

13637-84-8

fluorosulfonylchloride

33665-90-6

acetosulfam

Conditions
ConditionsYield
With sodium hydroxide; triethylamine In sulfur dioxide
55589-62-3

potassium acesulfame

33665-90-6

acetosulfam

Conditions
ConditionsYield
With hydrogenchloride In water pH=2;
With hydrogenchloride In water
With hydrogenchloride In water
With hydrogenchloride In water
With hydrogenchloride In water
33665-90-6

acetosulfam

55589-62-3

potassium acesulfame

Conditions
ConditionsYield
With potassium hydroxide In methanol pH=6.8; pH-value;97%
With potassium hydroxide In methanol; water at 35℃; Product distribution / selectivity;

copper (II) carbonate hydroxide

33665-90-6

acetosulfam

tetraaqua-bis(6-methyl-1,2,3-oxathiazin-4(3H)-onato-2,2-dioxide)copper(II)

Conditions
ConditionsYield
at 75℃; for 0.5h;95%
603-33-8

triphenylbismuthane

33665-90-6

acetosulfam

1422436-51-8

C14H13BiN2O8S2

Conditions
ConditionsYield
In diethyl ether at 20℃; for 4h; Temperature; Time;91.8%
33665-90-6

acetosulfam

72827-09-9

4-Chloro-6-methyl-[1,2,3]oxathiazine 2,2-dioxide

Conditions
ConditionsYield
With phosphorus pentachloride In tetrachloromethane Heating;90%
603-33-8

triphenylbismuthane

33665-90-6

acetosulfam

A

Bi(3+)*3C4H4NO4S(1-)

B

71-43-2

benzene

Conditions
ConditionsYield
In neat (no solvent) at 90℃; for 1h;A 86%
B n/a
2022-85-7

Flucytosine

33665-90-6

acetosulfam

2C4H4FN3O*C4H5NO4S

Conditions
ConditionsYield
at 20℃;
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    Name: Acesulfame Synonyms: 5,6-dimethyl-1,2,3-oxathiazin-4(3H)-one-2,2 dioxide CAS:33665-90-6 MF: C4H4KNO4S Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:Sweeteners Transport

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    Product Name: Acesulfame CAS: 33665-90-6 MF: C4H5NO4S MW: 163.15 EINECS: 251-622-6 Mol File: 33665-90-6.mol Acesulfame Structure Acesulfame Chemical Properties Melting point 123-123.5° density 1.83 pka -0.28±0

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  • 1,2,3-Oxathiazin-4(3H)-one,6-methyl-, 2,2-dioxide

  • Casno:

    33665-90-6

    1,2,3-Oxathiazin-4(3H)-one,6-methyl-, 2,2-dioxide

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Chemistry

Empirical Formula of Acesulfame (CAS NO.33665-90-6): C4H5NO4S
Molecular Weight: 163.1518 g/mol
EINECS: 259-715-3 
Index of Refraction: 1.514
Density: 1.512 g/cm3
Water solubility: 270 g/L at 20 °C
Structure of Acesulfame (CAS NO.33665-90-6):
                  
IUPAC Name: 6-Methyl-2,2-dioxooxathiazin-4-one
Canonical SMILES: CC1=CC(=O)NS(=O)(=O)O1
InChI: InChI=1S/C4H5NO4S/c1-3-2-4(6)5-10(7,8)9-3/h2H,1H3,(H,5,6)
InChIKey: YGCFIWIQZPHFLU-UHFFFAOYSA-N
Product Category of Acesulfame (CAS NO.33665-90-6): Biological buffer;Food sweetener agent;Food and feed additives

Uses

 Acesulfame (CAS NO.33665-90-6) can be used as sweetener in food, medicine or others.

Specification

 Acesulfame , its cas register number is 33665-90-6. It also can be called 6-Methyl-3,4-dihydro-1,2,3-oxathiazin-4-one 2,2-dioxide ; and 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide .