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3430-19-1

Basic Information
CAS No.: 3430-19-1
Name: 5-Methylpyridin-3-amine
Article Data: 11
Molecular Structure:
Molecular Structure of 3430-19-1 (5-Methylpyridin-3-amine)
Formula: C6H8N2
Molecular Weight: 108.143
Synonyms: 3-Picoline,5-amino- (7CI,8CI);(5-Methylpyridin-3-yl)amine;3-Amino-5-methylpyridine;5-Methyl-3-pyridinamine;
EINECS: 624-420-4
Density: 1.068 g/cm3
Melting Point: 59-63 °C
Boiling Point: 261.1 °C at 760 mmHg
Flash Point: 135.6 °C
Appearance: COLORLESS TO YELLOW SOLID
Hazard Symbols: ToxicT, IrritantXi, HarmfulXn
Risk Codes: 22-37/38-41-20/21/22
Safety: 26-36/37/39
PSA: 38.91000
LogP: 1.55340
Synthetic route
70-57-5

5-methylpyridinylcarboxamide

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
With potassium hydroxide; bromine 1.) RT, 1 h, 2.) 70 deg C, 15 min;67%
With sodium hydroxide; bromine In tetrahydrofuran at 5 - 70℃; Hoffmann rearrangement;
18344-51-9

2-amino-3-methyl-5-nitropyridine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
With hydrazine In water at 110 - 120℃; for 5h;45%
Multi-step reaction with 3 steps
1: calcium chloride; aqueous sodium nitrite solution; aqueous hydrochloric acid / Erhitzen des Reaktionsprodukts mit Wasser
2: phosphoryl chloride
3: palladium/charcoal; sodium acetate; acetic acid / Hydrogenation
View Scheme
Multi-step reaction with 2 steps
1: calcium chloride; aqueous sodium nitrite solution; aqueous hydrochloric acid / Erhitzen des Reaktionsprodukts mit Wasser
2: palladium/charcoal; sodium acetate; acetic acid / Hydrogenation
View Scheme
7598-26-7

5-Methyl-3-nitro-2-aminopyridine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
With hydrazine In water at 110 - 120℃; for 5h;41%
22280-56-4

2-chloro-3-methyl-5-nitropyridine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
With palladium on activated charcoal; sodium acetate; acetic acid Hydrogenation;
591-22-0

3,5-Lutidine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 27 percent / potassium permanganate / H2O / 1.) from RT to 43 deg C, 5 h, 2.) 45 deg C, overnight
2: thionyl chloride / Heating
3: ammonia gas / 1,2-dichloro-ethane / 0.5 h / -30 °C
4: 67 percent / bromine, aq. potassium hydroxide / 1.) RT, 1 h, 2.) 70 deg C, 15 min
View Scheme
3222-49-9

5-methylnicotinic acid

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: thionyl chloride / Heating
2: ammonia gas / 1,2-dichloro-ethane / 0.5 h / -30 °C
3: 67 percent / bromine, aq. potassium hydroxide / 1.) RT, 1 h, 2.) 70 deg C, 15 min
View Scheme
884494-95-5

5-methyl-nicotinic acid chloride

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: ammonia gas / 1,2-dichloro-ethane / 0.5 h / -30 °C
2: 67 percent / bromine, aq. potassium hydroxide / 1.) RT, 1 h, 2.) 70 deg C, 15 min
View Scheme
1603-40-3

3-methylpyridin-2-ylamine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: H2SO4; HNO3
2: calcium chloride; aqueous sodium nitrite solution; aqueous hydrochloric acid / Erhitzen des Reaktionsprodukts mit Wasser
3: phosphoryl chloride
4: palladium/charcoal; sodium acetate; acetic acid / Hydrogenation
View Scheme
Multi-step reaction with 3 steps
1: H2SO4; HNO3
2: calcium chloride; aqueous sodium nitrite solution; aqueous hydrochloric acid / Erhitzen des Reaktionsprodukts mit Wasser
3: palladium/charcoal; sodium acetate; acetic acid / Hydrogenation
View Scheme
21901-34-8

2-hydroxy-3-methyl-5-nitropyridine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: phosphoryl chloride
2: palladium/charcoal; sodium acetate; acetic acid / Hydrogenation
View Scheme
23132-21-0

2-bromo-3-methyl-5-nitropyridine

3430-19-1

5-methylpyridin-3-amine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol
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Chemistry

Molecule structure of 3-Amino-5-Methylpyridine (CAS NO.3430-19-1) :

IUPAC Name: (2S)-2-amino-3-(3-chloro-4-hydroxyphenyl)propanoic acid 
Molecular Weight: 215.6336 g/mol
Molecular Formula: C9H10ClNO3 
Density: 1.068 g/cm3
Melting Point: 59-63 °C 
Boiling Point: 261.1 °C at 760 mmHg 
Flash Point: 135.6 °C
Molar Volume: 101.2 cm3
Polarizability: 13.24*10-24 cm3
Surface Tension: 46.9 dyne/cm 
Enthalpy of Vaporization: 49.88 kJ/mol
Vapour Pressure: 0.0118 mmHg at 25 °C 
XLogP3: -1.8
H-Bond Donor: 3
H-Bond Acceptor: 4
Rotatable Bond Count: 3
Tautomer Count: 3
Exact Mass: 215.034921
MonoIsotopic Mass: 215.034921
Topological Polar Surface Area: 83.6
Heavy Atom Count: 14
Complexity: 212
Defined Atom StereoCenter Count: 1
Canonical SMILES: C1=CC(=C(C=C1CC(C(=O)O)N)Cl)O
Isomeric SMILES: C1=CC(=C(C=C1C[C@@H](C(=O)O)N)Cl)O
InChI: InChI=1S/C9H10ClNO3/c10-6-3-5(1-2-8(6)12)4-7(11)9(13)14/h1-3,7,12H,4,11H2,(H,13,14)/t7-/m0/s1
InChIKey: ACWBBAGYTKWBCD-ZETCQYMHSA-N
Product Categories of 3-Amino-5-Methylpyridine (CAS NO.3430-19-1) : VARIOUSAMINE; Heterocyclic Compounds; Amino; Intermediate; Pyridine; Boronic Acid; Heterocyclic Building Blocks; Pyridines; Building Blocks

Safety Profile

Hazard Codes: ToxicT, IrritantXi, HarmfulXn
Risk Statements: 22-37/38-41-20/21/22
R22: Harmful if swallowed
R37/38: Irritating to respiratory system and skin
R41:Risk of serious damage to the eyes 
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed
Safety Statements: 26-36/37/39-36
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection 
S36: Wear suitable protective clothing
Hazard Note: Toxic

Specification

 3-Amino-5-Methylpyridine (CAS NO.3430-19-1) is also called 3-Amino-5-picoline ; 5-Methyl-pyridin-3-ylamine ; 3-Amino-5-methylpyridine97% ; 3-Pyridinamine,5-methyl-(9CI) ; 5-Methyl-3-pyridylamine hydrochloride salt ; 5-Methyl-3-pyridinamine ; 5-Amino-3-methylpyridine .