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4151-50-2

Basic Information
CAS No.: 4151-50-2
Name: Sulfluramid
Article Data: 9
Molecular Structure:
Molecular Structure of 4151-50-2 (Sulfluramid)
Formula: C10H6F17NO2S
Molecular Weight: 527.202
Synonyms: AI 3-29757;Alstar;Alstar (pesticide);FX 12;FiniTron;GX 071;Mirex S;N-Ethylperfluorooctanesulfonamide;N-Ethylperfluorooctylsulfonamide;Volcano;Volcano (insecticide);
EINECS: 223-980-3
Density: 1.665 g/cm3
Melting Point: 75-85 °C
Boiling Point: 246.6 °C at 760 mmHg
Flash Point: 102.9 °C
Solubility: Insoluble (25 °C)
Appearance: Tan powder
Hazard Symbols: IrritantXi
Risk Codes: 21-22-51/53
Safety: 36/37-61
PSA: 54.55000
LogP: 6.36430
Synthetic route
307-35-7

perfluorooctyl sulfofluorure

75-04-7

ethylamine

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

Conditions
ConditionsYield
Stage #1: perfluorooctyl sulfofluorure; ethylamine With triethylamine In diethyl ether at 0 - 20℃; for 17h;
Stage #2: With sodium hydrogencarbonate In diethyl ether for 3h; Heating; Further stages.;
56%
In diethyl ether anhydr. ether, at -5 to 0°C, 2.75 h;
With triethylamine In di-isopropyl ether for 4h; Reflux;
In diethyl ether anhydr. ether, at -5 to 0°C, 2.75 h;
423-60-9

perfluorooctanesulphonyl chloride

75-04-7

ethylamine

A

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

B

N,N-dibutyl perfluorooctanesulfonamide

Conditions
ConditionsYield
In various solvent(s)A 0.05 mol
B 0.005 mol
423-60-9

perfluorooctanesulphonyl chloride

75-04-7

ethylamine

A

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

B

C8HF17O2S

C

C8HF17O2S*C2H7N

Conditions
ConditionsYield
In dichloromethane Product distribution; var. solv, investigated;
307-35-7

perfluorooctyl sulfofluorure

75-04-7

ethylamine

A

65756-36-7

hydrogen fluoride ethylamine

B

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

Conditions
ConditionsYield
In diethyl ether at -30-0°C,2.75 h;
In diethyl ether at -30-0°C,2.75 h;
4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

540-51-2

2-bromoethanol

1691-99-2

N-ethyl-N-(2-hydroxyethyl)-perfluorooctane-1-sulfonamide

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In acetone for 48h; Heating;99%
4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

102229-10-7

2-(tert-butyldimethylsilyloxy)ethanol

1017593-64-4

1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonic acid [2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-ethyl-amide

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In diethyl ether at 0 - 25℃; Mitsunobu reaction; sonication;98%
927-68-4

bromoethyl acetate

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

1017593-63-3

2-(N-ethyl-perfluorooctylsulfonamido)ethyl acetate

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In acetone for 36h; Heating;92%
4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

96-32-2

bromoacetic acid methyl ester

87988-69-0

methyl 2-(N-ethyl-perfluorooctanesulfonamido) acetate

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In acetone for 3h; Heating;90%
108-77-0

1,3,5-trichloro-2,4,6-triazine

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

N-(4,6-dichloro-1,3,5-triazin-2-yl)-N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

Conditions
ConditionsYield
Stage #1: N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide With sodium In ethanol for 0.5h; Metallation;
Stage #2: 1,3,5-trichloro-2,4,6-triazine In acetone at -78 - 20℃; for 2h; Substitution;
72%
96-35-5

glycolic acid methyl ester

4151-50-2

N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide

87988-69-0

methyl 2-(N-ethyl-perfluorooctanesulfonamido) acetate

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In diethyl ether at 0 - 25℃; Mitsunobu reaction; sonication;67%
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    Sulfluramid

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    Chemical Name Sulfluramid Synonyms N-Ethyl perfluorooctanesulfonamide; N-Ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-octanesulfonamide;FX-9 CAS No. 4151-50-2

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    4151-50-2

    1-Octanesulfonamide,N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-

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Chemistry

Empirical Formula: C10H6F17NO2S
Molecular Weight: 527.198 g/mol
EINECS: 223-980-3
Index of Refraction: 1.32
Density: 1.665 g/cm3
Flash Point: 102.9 °C
Melting point: 75-85 °C
Appearance: Tan powder
Enthalpy of Vaporization: 48.37 kJ/mol
Boiling Point: 246.6 °C at 760 mmHg
Vapour Pressure: 0.0269 mmHg at 25 °C
Structure of Sulfluramid (CAS NO.4151-50-2):
                   
IUPAC Name: N-Ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluorooctane-1-sulfonamide
Product Category of Sulfluramid (CAS NO.4151-50-2): Organics;Sulfur & Selenium Compounds;Pesticide & intermediate;Metal Isotopes

Uses

 Sulfluramid (CAS NO.4151-50-2) can be used as emulsifier, wetting agent, and organic fluorine.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
quail LD50 oral 473mg/kg (473mg/kg)   Pesticide Manual. Vol. 9, Pg. 773, 1991.
rat LD50 oral 543mg/kg (543mg/kg)   Pesticide Manual. Vol. 9, Pg. 773, 1991.

Safety Profile

Hazard Codes: IrritantXi
Hazard Note: Irritant

Specification

 Sulfluramid , its cas register number is 4151-50-2. It also can be N-Ethyl perfluorooctanesulfonamide ; and N-Ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-octanesulfonamide .