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656247-17-5

Basic Information
CAS No.: 656247-17-5
Name: Nintedanib
Article Data: 30
Molecular Structure:
Molecular Structure of 656247-17-5 (Nintedanib)
Formula: C31H33N5O4
Molecular Weight: 539.634
Synonyms: Vargatef;
EINECS: 1592732-453-0
Density: 1.284g/cm3
Boiling Point: 742.199°C at 760 mmHg
Flash Point: 402.667°C
PSA: 94.22000
LogP: 3.70270
Synthetic route
656247-18-6

methyl (3Z)-3-[({4-[N-methyl-2-(4-methylpiperazin-1-yl)acetamido]phenyl}amino)(phenyl)methylidene]-2-oxo-2,3-dihydro-1H-indole-6-carboxylate ethanesulfonate salt

656247-17-5

nintedanib

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; ethyl acetate at 40℃; for 1h;98.7%
With sodium carbonate In water pH=9; Solvent; pH-value;20 g
262368-30-9

N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine

1168152-07-5

(E)-1-acetyl-3-(methoxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester

656247-17-5

nintedanib

Conditions
ConditionsYield
Stage #1: N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine; (E)-1-acetyl-3-(methoxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester With methanol In N,N-dimethyl-formamide at 75℃; for 4h; Large scale;
Stage #2: With methanol; potassium hydroxide In N,N-dimethyl-formamide Temperature; Large scale;
94.6%
Stage #1: N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine; (E)-1-acetyl-3-(methoxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester In methanol for 5h; Reflux;
Stage #2: With potassium hydroxide In methanol at 20 - 70℃; for 0.5h; Concentration; Reagent/catalyst; Temperature; Solvent;
90%
Stage #1: N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine; (E)-1-acetyl-3-(methoxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester In methanol; N,N-dimethyl-formamide Reflux;
Stage #2: With piperidine In methanol; N,N-dimethyl-formamide Reflux;
88%
Stage #1: N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine; (E)-1-acetyl-3-(methoxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester In methanol for 5h; Reflux;
Stage #2: With potassium hydroxide In methanol
84%
Stage #1: N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine; (E)-1-acetyl-3-(methoxy-phenyl-methylene)-2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester In N,N-dimethyl-formamide at 80℃; for 1h;
Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 2h;
77%
109-01-3

1-methyl-piperazine

methyl 1-acetyl-3-(((4-(2-chloro-N-methylacetamido)phenyl)amino)(phenyl)methylene)-2-oxoindoline-6-carboxylate

656247-17-5

nintedanib

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 45 - 50℃;93.74%
109-01-3

1-methyl-piperazine

methyl-1-acetyl-3-((4-(2-chloro-N-ethylacetamido)phenyl)amino(phenyl)methylene)-2-oxoindoline-6-carboxylate

656247-17-5

nintedanib

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 45 - 50℃;93.74%
109-01-3

1-methyl-piperazine

C26H22ClN3O4

656247-17-5

nintedanib

Conditions
ConditionsYield
In toluene at 65℃; for 4h; Solvent; Temperature;93%
262368-30-9

N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine

methyl 3-[bromo(phenyl)methylidene]-2-oxoindoline-6-formate

656247-17-5

nintedanib

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethanol for 2h; Reflux;92.7%
262368-30-9

N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine

methyl 1-acetyl-3-[methoxy(phenyl)methylidene]-2-oxo-2,3-dihydro-1H-indole-6-carboxylate

656247-17-5

nintedanib

Conditions
ConditionsYield
With pyrrolidine In methanol at 25 - 50℃; for 6h;91.37%

1-acetyl-3-(Z)-[1-(4-(N-((4-methylpiperazin-1-yl)methylcarbonyl)-N-methylaminophenyl)amino)-1-phenylmethylene]-6-methoxycarbonyl-2-indolinone

656247-17-5

nintedanib

Conditions
ConditionsYield
With methanol; potassium hydroxide at 20℃; Reagent/catalyst; Large scale;91.3%
With methanol; potassium hydroxide at 50 - 55℃; for 2h; Temperature;
262368-30-9

N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine

1168150-46-6

(E)-methyl 3-(methoxy(phenyl)methylene)-2-indolone-6-carboxylic acid methyl ester

656247-17-5

nintedanib

Conditions
ConditionsYield
In methanol for 8h; Reflux;90.8%
93-58-3

benzoic acid methyl ester

262368-30-9

N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine

14192-26-8

2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester

656247-17-5

nintedanib

Conditions
ConditionsYield
Stage #1: benzoic acid methyl ester; 2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 3h;
Stage #2: N-[(4-methyl-piperazin-1-yl)methylcarbonyl]-N-methyl-p-phenylendiamine In N,N-dimethyl-formamide at 20℃; for 4h;
89.7%
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    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

  •  Afine Chemicals Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • Vargatef

  • Casno:

    656247-17-5

    Vargatef

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • Nintedanib

  • Casno:

    656247-17-5

    Nintedanib

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Nintedanib is one of the most competitive products in our company, we can supply it with good quality and best price. Appearance:Yellow to brown solid Storage:Room temperature, Keep in Dark Place. Package:According to the demand of customer Applicati

    Nanjing Fred Technology Co.,Ltd. is a Fine Chemicals Company, specializing in research, development, manufacture and distribute raw materials for pharmaceutical, healthcare, bioc

  •  Nanjing Fred Technology Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-25-84696168

    Address:Nanjing

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  • BIBF1120 Nintedanib 656247-17-5

  • Casno:

    656247-17-5

    BIBF1120 Nintedanib 656247-17-5

    Min.Order: 5 Gram

    FOB Price:  USD $ 0.0-0.0

    Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

    Taizhou Crene Biotechnology Co., Ltd.is a leading supplier of active pharmaceutical ingredients (APIs), with GLP labs and GMP manufacturing facilities engaging in organic synthesis

  •  Taizhou Crene Biotechnology co.ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-576-88813233 88205808

    Address:Economic Developed Zone of Taizhou Zhejiang China

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  • Nintedanib

  • Casno:

    656247-17-5

    Nintedanib

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

    Hangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service profession

  •  Hangzhou Keyingchem Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85378921

    Address:Jintong international Building, No.113,Huayuangang Street, Gong shu District, Hangzhou,Zhejiang, China.

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  • Intedanib

  • Casno:

    656247-17-5

    Intedanib

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1. Product advantages: exquisite appearance and unique functions. 2. Product Advantages: Our products are the best,fast speed ,in large stock 3. High-quality products and thoughtful service are your greatest satisfaction. 4. The product

    Shanghai Hope Chem Co., Ltd. was founded in 2014 with registered capital of RMB 2 million Yuan. Our company is specialized in the researching, discovering and manufacturing of new

  •  Shanghai Hope Chem Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-21-58090396-805

    Address:Floor 4, Building 5, No.588 Tianxiong Road, Zhoupu International Medical Zone, ShangHai, China

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  • Nintedanib/High quality/Best price

  • Casno:

    656247-17-5

    Nintedanib/High quality/Best price

    Min.Order: 1 Gram

    FOB Price:  USD $ 1.0-1.0

    Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

    Shanghai Massive Chemical Technology Co., Ltd. is engaged in development, production and marketing Specialty Chemicals to satisfy the changing needs of the chemical industry. We sp

  •  Shanghai Massive Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 21 34943721

    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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  • High quality Nintedanib

  • Casno:

    656247-17-5

    High quality Nintedanib

    Min.Order: 10 Gram

    FOB Price:  USD $ 100.0-100.0

    Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

    Hangyu Biotech is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and O

  •  Zibo Hangyu Biotechnology Development Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15965530500

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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  • Nintedanib

  • Casno:

    656247-17-5

    Nintedanib

    Min.Order: 100 Gram

    FOB Price:  USD $ 100.0-2000.0

    We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

    SHANGHAI SYSTEAM BIOCHEM CO., LTD. is one of the professional suppliers in Chinese pharmaceutical market and is specialized in custom synthesis, chemical/pharmaceutical/ pesticides

  •  SHANGHAI SYSTEAM BIOCHEM CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-021-58380978

    Address:Building 87,Lane 669, Dong Jing Road Shanghai,P.R.China

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  • Nintedanib

  • Casno:

    656247-17-5

    Nintedanib

    Min.Order: 10 Gram

    FOB Price:  USD $ 0.0-0.0

    Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

    TaiChem was established in 2015 and registered in China medical city - Taizhou, Jiangsu Province. The company has about 1800 square meters of class A plant facility. TaiChem focuse

  •  TaiChem Taizhou Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-0523-86810091

    Address:Changjiang Dadao 18

       Inquiry Now

  • Best Quality Nintedanib

  • Casno:

    656247-17-5

    Best Quality Nintedanib

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Product name: Nintedanib CAS No.:656247-17-5 Molecule Formula:C31H33N5O4 Molecule Weight:539.62 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS

    Siwei Development Group Ltd. is a reputed professional enterprise in China dedicated to the Amino Acids production and sales of fine chemical products.Over the years we have been m

  •  Siwei Development Group Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-571-82881840

    Address:Rm2-2-503 Zhongdingyuan, Xianghurenjia Wenyan Xiaoshan, Hangzhou China

       Inquiry Now

  • In Bulk SupplyNintedanib

  • Casno:

    656247-17-5

    In Bulk SupplyNintedanib

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

    Jiangsu Qianyu Molecular Technology Co., LTD. Jiangsu Qianyu Molecular Technology is a high-tech medical and health enterprise,located in a developed transportation city Xuzhou, Ch

  •  Jiangsu Qianyu Molecular Technology Co., LTD.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 18652199763

    Address:No.2-812, Zhongyin Plaza,Yunlong District

       Inquiry Now

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