119124-12-8Relevant articles and documents
ACETONITRILE: AN EXCELLENT SOLVENT FOR THE 1,1-DICHLOROMETHYLENATION OF CERTAIN KETONES
Burton, George,Elder, John S.,Fell, Stephen C. M.,Stachulski, Andrew V.
, p. 3003 - 3006 (2007/10/02)
Cyclohexanones react rapidly at or below room temperature with Ph3P and XCCl3 (X=Br or Cl) in acetonitrile to give 1,1-dichloromethylenecompounds in high yield; some α-methoxyimino β-(1,1-dichloro)methylene esters have been similarly prepared.