145701-21-9Relevant articles and documents
HERBICIDAL COMPOSITIONS
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, (2022/03/02)
The present invention provides compositions comprising herbicidally active compounds (A) and (B), where (A) represents one or more compounds of the general formula (I) or agrochemically compatible salts thereof [component (A)], and (B) represents one or more herbicides [component (B)]. The application further relates to a method and to the use of the herbicidal composition according to the invention for controlling harmful plants or for regulating growth.
The preparation method of the double chlorine sulphur grass amine (by machine translation)
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Paragraph 0014; 0015; 0016; 0018; 0019; 0020, (2017/07/21)
The invention discloses a double-chlorine sulphur grass amine preparation method, which is composed of a 2 - chloro sulfonyl - 7 - fluoro - 5 - ethoxy [1, 2, 4] triazolo [1, 5 - c] pyrimidine in organic solvent with 2, 6 - dichloro the amine passes through condensation reaction; said condensation reaction is 3, 5 - dimethyl pyridine carried out under catalysis. The 2 - chloro sulfonyl - 7 - fluoro - 5 - ethoxy [1, 2, 4] triazolo [1, 5 - c] pyrimidine with the 3, 5 - dimethyl pyridine molar ratio of 1:1 - 1:5. Said organic solvent is dimethyl sulfoxide (DMSO) containing mixed solvent; the mixed solvent of dimethyl sulfoxide in a weight percentage of 0.1% -1%. The method of the invention is high in safety, simple operation, simple process conditions, in particular by selection of appropriate catalyst and organic solvent, can obtain higher reaction yield and purity of the product, is suitable for industrial production. (by machine translation)
N-ARYLSULFILIMINE COMPOUNDS AND THEIR USE AS CATALYSTS IN THE PREPARATION OF N-ARYLARYLSULFONAMIDE COMPOUNDS
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, (2008/06/13)
N-arylsulfilimine compounds, such as S,S-dimethyl-N-(2,6-dichlorophenyl)sulfilimine, were prepared and found to catalyze the reaction of aromatic sulfonyl chloride compounds, such as 2-chlorosulfonyl-7-fluoro-5-ethoxy[1,2,4]triazolo[1,5-c]pyrimidine, with aromatic amine compounds, such as 2,6-dichloroaniline, to form N-arylarylsulfonamide compounds, such as N-(2,6-dichlorophenyl)-7-fluoro-5-ethoxy[1,2,4]triazolo[1,5-c]-pyrimidine-2-sulfonamide. The aryl moiety of the N-arylsulfilimine catalyst and the aryl moiety of the aromatic amine compound were generally chosen to be identical.