15057-15-5Relevant articles and documents
A practical and scalable process to selectively monofunctionalize water-soluble α,ω-diols
Zhang, Quanxuan,Ren, Hong,Baker, Gregory L.
supporting information, p. 3384 - 3386 (2014/06/09)
A practical protocol for rapid and scalable synthesis of monofunctionalized α,ω-diols using a simple and inexpensive THP ether protection/deprotection strategy was described. Use of inexpensive DHP source and ease to remove excess water-soluble α,ω-diols
Difunctionalized Trans-2,5-Disubstituted Pyrrolidine (Azethoxyl) Nitroxide Spin-Labels
Keana, John F. W.,Seyedrezai, Seyed E.,Gaughan, Glen
, p. 2644 - 2647 (2007/10/02)
The synthesis of two short-chain trans-2,5-difunctionalized azethoxyl nitroxide spin-labels, dinitrile 12 and dicarboxylic acid 14, is described.The trans stereochemistry of 12 and 14 was established by conversion of 12 to a diastereomeric mixture of N-hydroxy esters 13, which was analyzed by NMR spectroscopy.