15088-77-4Relevant articles and documents
Catalyst- and organic solvent-free synthesis of thioacids in water
Elagawany, Mohamed,Hegazy, Lamees,Elgendy
, p. 2018 - 2021 (2019)
Thioacids and thioamino acids were synthesized in excellent yields from readily available acyl benzotriazoles and sodium hydrosulfide in water at room temperature. The new methodology features mild reaction conditions, high yields, short reaction times, and does not involve the use of organic solvents or bases. The reaction is eco-friendly, and the workup procedure is simple and does not require chromatographic separation.
A facile method for the synthesis of diacyl disulfides
Jia, Xue-Shun,Liu, Xiao-Tao,Li, Qing,Huang, Qing,Kong, Ling-Long
, p. 547 - 548 (2007/10/03)
A facile method for the synthesis of diacyl disulfides is reported. Sulfur is reduced with samarium diiodide at room temperature to give samarium disulfides, which react with acyl chlorides in the presence of HMPA to afford the corresponding diacyl disulfides in high yields.
A convenient method for the synthesis of diacyl disulfides
Wang,Cui,Hu,Zhao
, p. 889 - 898 (2007/10/02)
A simple and general method for the synthesis of diacyl disulfides is reported. Sulfur is allowed to react with sodium hydroxide to give sodium disulfide at 65°C under PTC, which can react with acyl halides to afford diacyl disulfides in good to excellent isolated yields. The effects of solvents and phase transfer catalysts are discussed.
