1630-09-7

Basic information

• Product Name: 1,3-DICHLORO-2,4,6-TRINITROBENZENE
• Synonyms: 1,3-DICHLORO-2,4,6-TRINITROBENZENE;2,4-DICHLORO-1,3,5-TRINITROBENZENE
• CAS NO: 1630-09-7
• Molecular Formula: C₆HCl₂N₃O₆
• Molecular Weight: 281.99
• Mol File: 1630-09-7.mol
• Article Data: 5

Chemical Properties

• Melting Point: 126.5-127 °C
• Boiling Point: 380 °C at 760 mmHg
• Flash Point: 183.6 °C
• Appearance: /
• Density: 1.894g/cm³
• Vapor Pressure: 1.23E-05mmHg at 25°C
• Refractive Index: 1.671
• CAS DataBase Reference: 1,3-DICHLORO-2,4,6-TRINITROBENZENE(CAS DataBase Reference)
• NIST Chemistry Reference: 1,3-DICHLORO-2,4,6-TRINITROBENZENE(1630-09-7)
• EPA Substance Registry System: 1,3-DICHLORO-2,4,6-TRINITROBENZENE(1630-09-7)

Safety Data

• Hazardous Substances Data: 1630-09-7(Hazardous Substances Data)

Usage

Synthesis Reference(s)

The Journal of Organic Chemistry, 26, p. 2997, 1961 DOI: 10.1021/jo01066a613

InChI:InChI=1/C6HCl2N3O6/c7-4-2(9(12)13)1-3(10(14)15)5(8)6(4)11(16)17/h1H

Upstream product

• 1706-82-7 3-chloro-2,4,6-trinitro-phenol 
• 98-59-9 p-toluenesulfonyl chloride 
• 75-44-5 phosgene 
• 3698-60-0 dipyridinium styphnate 
• 82-71-3 styphnic acid 
• 601-88-7 2,6-dichloronitrobenzene 
• 10199-85-6 1-chloro-2,4-dinitrochlorobenzene 
• 60764-03-6 3-chloro-2,4,6-trinitro-phenol; potassium-(3-chloro-2.4.6-trinitro-phenolate) 
• 21212-69-1 1-bromo-3-methoxy-2,4,6-trinitrobenzene 
• 2845-90-1 chloromethoxy-1,3,5-trinitrobenzene 
• 3698-60-0 pyridine; compound with 2,4,6-trinitro-resorcinol 
• 541-73-1 1,3-Dichlorobenzene 
• 3698-83-7 2,4-dichloro-1,5-dinitrobenzene 

Downstream Products

• 409322-65-2 N,N'-(2,4,6-trinitro-m-phenylene)-bis-glycine 
• 97827-67-3 2,4,6-Trinitro-1,3-bis-<4-acetyl-anilino>-benzol-dioxim 
• 95559-62-9 2.4.6.-Trinitro-1.3-bis-<4-methyl-anilino>-benzol 
• 7629-69-8 2-[N'-(3-chloro-2,4,6-trinitro-phenyl)-N-phenyl-hydrazino]-benzothiazole 
• 14770-31-1 4,4'-diphenyl-2,2'-[N,N''-diphenyl-N',N'''-(2,4,6-trinitro-m-phenylene)-dihydrazino]-bis-thiazole 
• 784-12-3 2,4-Difluor-1,3,5-trinitro-benzol 
• 1202166-11-7 4,4'-(2,4,6-trinitro-1,3-phenylene)bis(oxy)bis(3-nitrofurazan) 
• 108950-83-0 piperonal-(3-chloro-2,4,6-trinitro-phenylhydrazone) 
• 117869-08-6 formaldehyde-(3-chloro-2,4,6-trinitro-phenylhydrazone) 
• 409322-90-3 N,N'-dinitro-N,N'-(2,4,6-trinitro-m-phenylene)-bis-glycine 
• 858255-71-7 N,N'-dinitro-N,N'-(2,4,6-trinitro-m-phenylene)-bis-glycyl chloride 
• 85950-48-7 3-amino-1,5-dihydroxy-2,4-dimethoxybenzene hydrochloride 
• 71479-92-0 5,7-dihydroxy-3,6,8-trimethoxyflavone 
• 85950-47-6 N-(5-Acetylamino-3-amino-2,4-dimethoxy-phenyl)-acetamide 

Relevant articles and documents

Synthesis of 1,3-bis(1,2,4-triazol-3-amino)-2,4,6-trinitrobenzene and its thermal and explosive behaviour

1,3-Bis(1,2,4-triazol-3-amino)-2,4,6-trinitrobenzene (BTATNB) has been synthesized by condensing 1,3-dichloro-2,4, 6-trinitrobenzene and 3-amino-1,2,4-triazole in dimethyl formamide (DMF) at 125 ± 2 °C. The product has been characterized by elemental analysis, Fourier transform infrared (FTIR), nuclear magnetic resonance (NMR) and mass spectrometry. The data on thermal and explosive properties indicate that BTATNB is slightly more thermally stable than 3-picrylamino-1,2,4-triazole (PATO). At the same time, it is safer towards impact and friction.

REPLACEMENT OF REACTIVE PHENOLIC HYDROXYL GROUPS BY CHLORINE WITH

-

Chloro- and bromo-demethoxylation of methoxypolynitroaryl systems

Various reagents for effecting halogenodemethoxylation of methoxy substituted polynitrophenyl and -biphenyl systems have been investigated, and the preferred procedures for achieving chloro- and bromo-demethoxylation in high yield have been identified.