17212-17-8Relevant articles and documents
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Nelson,Percival
, p. 2191 (1957)
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Structural analysis of the O-polysaccharide of the lipopolysaccharide from Azospirillum brasilense Jm6B2 containing 3-O-methyl-D-rhamnose (D-acofriose)
Boyko, Alevtina S.,Dmitrenok, Andrey S.,Fedonenko, Yuliya P.,Zdorovenko, Evelina L.,Konnova, Svetlana A.,Knirel, Yuriy A.,Ignatov, Vladimir V.
experimental part, p. 92 - 95 (2012/09/07)
Two types of neutral O-polysaccharides were obtained by mild acid degradation of the lipopolysaccharide isolated by phenol-water extraction from the asymbiotic diazotrophic rhizobacterium Azospirillum brasilense Jm6B2. The following structure of the major O-polysaccharide was established by composition and methylation (ethylation) analyses, Smith degradation, and 1D and 2D 1H and 13C NMR spectroscopy: α-D-Rhap3OMe 1↓3→4)-α-L-Fucp-(1→4)-β-D-Xylp-(1→ where a non-stoichiometric (~60%) 3-O-methylation of D-rhamnose is indicated by italics.