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Preparation method of methylphenylvinylethoxysilane
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Paragraph 0029; 0030, (2016/12/01)
The invention relates to the field of organic chemistry and discloses a preparation method of methylphenylvinylethoxysilane. The preparation method solves the problem that the existing Grignard method for preparing methylphenylvinylethoxysilane has harsh reaction conditions, has large reaction control difficulty, produces more side products, utilizes an ether solvent and easily produces explosion in ether solvent recovery because of peroxide production in ether solvent recovery. The preparation method utilizes methylvinylethoxysilane and chlorobenzene as raw materials and a sodium condensation method to prepare methylphenylvinylethoxysilane. The preparation method has mild reaction conditions, utilizes raw materials as solvents, has simple processes and is very suitable for large scale production.