181178-76-7Relevant articles and documents
The facile synthesis of O,O-dialkyl α-halobenzylphosphonates from O,O-dialkyl α-hydroxybenzylphosphonates
Green, Donovan,Elgendy, Said,Patel, Geeta,Baban, Jehan A.,Skordalakes, Emmanuel,Husman, Wahid,Kakkar, Vijay V.,Deadman, John
, p. 10215 - 10224 (2007/10/03)
O,O-dialkyl α-hydroxybenzylphosphonates (1) can be easily converted in their corresponding α-bromo (2) or α-iodo (3) phosphonates, in quantitative yield, using N,N'-carbonyldiimidazole (CDI) in the presence of allyl bromide or methyl iodide.