18279-67-9Relevant articles and documents
Process for preparing low-chloride or chloride-free alkoxysilanes
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, (2008/06/13)
A process for preparing an alkoxysilane with an acidic chloride content of less than 10 ppm by weight, comprising: reacting a chlorosilane with an alcohol in a water-free and solvent-free phase to form a product mixture containing alkoxysilane and residual acidic chloride, with removal of resultant hydrogen chloride from the product mixture, then adding liquid or gaseous ammonia, in an amount corresponding to a stoichiometric excess, based on the content of acidic chloride, to form an ammonia-containing product mixture, treating the ammonia-containing product mixture at a temperature between 10 and 50 DEG C., wherein the ammonia and acidic chloride undergo neutralization, to form a crude product, and optionally, then separating off a salt formed in the course of neutralization, from the crude product, and recovering the alkoxysilane by distilling the crude product.
Process for the production of alkoxy-β-halogenoethylsilanes
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, (2008/06/13)
A process for the production of trialkoxy-β-halogenoethylsilanes and dialkoxy-methyl-β-halogenoethylsilanes by reaction of a corresponding β-halogenoethyltrichlorosilane or β-halogenoethyl-methyldichlorosilane with an alcohol in the presence of ammonia is disclosed. The trialkoxy-β-halogenoethylsilanes and dialkoxy-methyl-β-halogenoethylsilanes obtained by this process are active substances for regulating plant growth.
