19622-69-6Relevant articles and documents
Synthesis and stability of [1,3-14C2]-glyceryl trinitrate
Szammer,Simon-Trompler,Mate,Abermann,Klebovich
, p. 1111 - 1115 (1994)
The synthesis of [1,3-14C2]-glyceryl trinitrate ([14C]-GTN) labelled with quasi carrier free carbon-14 atom in the 1,3-positions of the molecule was effected in four reaction steps from 14CO2 ( 3,5% overall yield). The chemical and radiochemical purity of [14C]-GTN was found better than 99% controlled by HPLC-Radioactivity Monitor and TLC-Digital Autoradiograph methods. Study of the radiochemical stability in dilute solution at 5 °C shows l:hat the product can be stored at least for a month without detectable decomposition.
