20108-67-2Relevant articles and documents
Efficient acylation and one-pot synthesis of dehydroandrographolide succinate on a large scale assisted with microwave radiation
Luo, Xin-Feng,He, Ling,Yin, Hai-Bin,Zheng, Hu,Bei, Di,Deng, Jin-Jin,Huang, Wen-Cai
experimental part, p. 3444 - 3452 (2009/12/05)
A rapid and convenient method for acylation and large-scale synthesis of dehydroandrographolide succinate has been developed under microwave irradiation. It is a one-pot condensation and is compatible with dehydration and rearrangement of double bond in mild reaction conditions with good yield, high purity (up to 99.8%), time-savings, few pollutants and low cost. In addition, a number of acylation derivatives were synthesized under microwave irradiation.
The structure of adenomycin (C19-97 substance)
Ogita,Otake,Miyazaki,et al.
, p. 3203 - 3206 (2007/10/02)
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