208343-47-9Relevant articles and documents
Preparation method of triazines UV absorbent
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Paragraph 0073-0079; 0083-0085, (2019/03/08)
The invention relates to a preparation method of 2,4-bi(2-hydroxy-4-butylphenyl)-6-(2,4-dibutylphenyl)-1,3,5-triazine. The method comprises the following steps: (10 carrying out a reaction between cyanuric chloride and resorcinol under the effect of a combined immobilized catalyst to generate a component I which is 2,4, 6-tri(2,4-dihydroxyphenyl)-1, 3, 5-triazine; (2) carrying out a reaction of the compound as shown in formula I and butyl halide under the effects of a phase transfer catalyst and an alkaline solution to obtain the target compound. The method has the following advantages: (1) the combined immobilized catalyst is used and the separation technology of reaction materials is simplified, and the separating effect can be realized by simply filtering the solid catalyst, and thus alarge number of aluminum salt containing acidic wastewater can be decreased; (2) the phase transfer catalyst is used for catalyzing the esterifying reaction, and the process is simplified, a severe anhydrous condition is avoided; compared with traditional Williamoson esterifying reaction, the method has the advantage that a large number of compound salt wastes which are hard to separate can be decreased.