22396-72-1Relevant articles and documents
Copper- and amine-free Sonogashira reaction of N,N-disubstituted propargylamine: Synthesis of substituted aryl propargylamine
Zhang, Weiwei,Cheng, Jiang,Ding, Linya,Zhong, Ping,Zhao, Li,Wu, Huayue
, p. 2001 - 2007 (2006)
A copper- and amine-free Sonogashira reaction of N,N -disubstituted propargylamine (DEP) is reported. The procedure was mild and tolerated a series of aryl bromides, affording the substituted aryl propargylic amines in good to excellent yield. Copyright T
Microwave-promoted, solvent-free, three-component coupling of aldehyde, alkyne, and amine catalyzed by AgNO3
He, Tingting,Zha, Zhenggen,Pan, Chongfeng,Wang, Zhiyong
, p. 849 - 858 (2007)
An efficient three-component coupling reaction of alkyne, aldehyde, and amine was carried out in one pot smoothly under the catalysis of AgNO3 and microwave irradiation. The scope of reaction substrates was extended. Moreover, the reaction can be performe
Synthesis, characterization and catalytic properties of cationic N-heterocyclic carbene silver complexes
Atli, Deniz Demir
, p. 577 - 584 (2021/07/26)
Three new dibenzimidazolium salts bridged by 2-methylenepropane-1,3-diyl group were synthesized. Their dinuclear N-heterocyclic carbene Ag(I) complexes were prepared by the reactions of these salts with Ag2O. The structures of the synthesized compounds were defined by nuclear magnetic resonance (NMR), Fourier-transform infrared spectroscopy (FT-IR), elemental analysis, and LC-MSMS (for complexes) techniques. Stability of the silver complexes was confirmed by 1H NMR spectroscopy. Catalytic activities of Ag(I) compounds were tested for three-component coupling reaction of some aldehydes, amines, and phenylacetylene.
Nano and Sub-nano Gold–Cobalt Particles as Effective Catalysts in the Synthesis of Propargylamines via AHA Coupling
Bensaad, Meriem,Berrichi, Amina,Bachir, Redouane,Bedrane, Sumeya
, p. 1068 - 1079 (2020/09/11)
Abstract: Titania supported Au–Co catalysts with nano- and sub-nanoparticles, were prepared with 1% Au and different contents of cobalt by one pot deposition precipitation with urea. Monometallic gold and cobalt catalysts were also prepared by the same me