22452-72-8

Basic information

• Product Name: 3,3'-thiodibenzoic acid
• Synonyms: 3,3'-thiodibenzoic acid
• CAS NO: 22452-72-8
• Molecular Weight: 274.297
• Mol File: 22452-72-8.mol
• Article Data: 3

Chemical Properties

• CAS DataBase Reference: 3,3'-thiodibenzoic acid(CAS DataBase Reference)
• NIST Chemistry Reference: 3,3'-thiodibenzoic acid(22452-72-8)
• EPA Substance Registry System: 3,3'-thiodibenzoic acid(22452-72-8)

Safety Data

• Hazardous Substances Data: 22452-72-8(Hazardous Substances Data)

Upstream product

• 618-51-9 3-Iodobenzoic acid 

Downstream Products

• 131073-61-5 3-[(3-carboxyphenyl)sulfinyl]benzenecarboxylic acid 

Relevant articles and documents

Copper(II)-Catalyzed Single-Step Synthesis of Aryl Thiols from Aryl Halides and 1,2-Ethanedithiol

A highly efficient transition metal-catalyzed single-step synthesis of aryl thiols from aryl halides has been developed employing copper(II) catalyst and 1,2-ethanedithiol. The key features are use of readily available reagents, a simple operation, and relatively mild reaction conditions. This new protocol shows a broad substrate scope with excellent functional group compatibility. A variety of aryl thiols are directly prepared from aryl halides in high yields. Furthermore, the aryl thiols are used in situ for the synthesis of more advanced molecules such as diaryl sulfides and benzothiophenes.

3-Mercaptopropionic Acid: A New Tool in the Synthesis of Symmetrical Diaryl Sulfides from Unactivated Aryl Iodides as Substitute for Anhydrous Sodium Sulfide

A series of symmetrical diaryl sulfides has been prepared by the copper-catalyzed reaction of 3-mercaptopropionic acid with unactivated aryl iodides.The yields are comparable with those obtained using anhydrous sodium sulfide under optimized reaction conditions.