23459-55-4Relevant articles and documents
Ligand-free Cu(ii)-mediated aerobic oxidations of aldehyde hydrazones leading to N,N′-diacylhydrazines and 1,3,4-oxadiazoles
Liu, Lei,Feng, Suliu
supporting information, p. 2585 - 2592 (2017/04/03)
A Cu(ii)-mediated synthesis of N,N′-diacylhydrazines and 1,3,4-oxadiazoles from aldehyde hydrazones has been developed. This is the first time that the synthesis of N,N′-diacylhydrazines and 1,3,4-oxadiazoles using N,N-dimethylamides as the acylation reagent and O2 in air as the oxidation reagent is reported. These reactions offered several advantages including simple workups, ligand-free inexpensive metal salts as mediators, high yields, and wide scope of substrates.
Acylation Reactions of Phenylhydrazines. Preparation and Properties of New Diacylphenylhydrazines
Hearn, Michael J.,Magee, Debra J.,Alhart, Randi,Gleva, Marye,Goldstein, Susan,et al.
, p. 129 - 131 (2007/10/02)
Anhydride acylation reactions of a variety of substituted arylhydrazines under mild conditions led to controlled formation of the acid phenylhydrazides I (Table I).The procedures were tallored to the particular state of the starting arylhydrazine.Second-s