28694-04-4Relevant articles and documents
Preparation method of 1,4- dibenzylidene malonic ester (by machine translation)
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Paragraph 0033-0034, (2019/12/11)
The preparation method comprises the following 1,4 - steps: dissolving the terephthalaldehyde and the malonate of the formula in 1 an organic solvent; reacting 2 under the action of a catalyst; and after the reaction is 20 - 80 °C complete, the method comprises the following 3 steps 1,4 - reacting with organic acid and organic base; and reacting the reaction route as follows. In-flight vehicle R1 Sum-up table R2 An alkyl, alkenyl or 1 - 18 alkynyl group is independently selected from alkyl, alkenyl or alkynyl groups containing from about. The method provided by the invention is simple in process, short in flow, mild in reaction conditions, high in conversion rate, and capable of recycling and recycling auxiliary materials such as solvents. (by machine translation)