43100-26-1Relevant articles and documents
Synthesis of acylhydrazines and, symmetrical and asymmetrical diacylhydrazines from carboxylic acid via the Vilsmeier reagent mediated process
Zarei, Maaroof,Nakhli, Maliheh Eslami
, p. 1909 - 1918 (2017/02/15)
(Chloromethylene)dimethylammonium chloride (Vilsmeier reagent) has been used as an efficient and convenient reagent for the one-pot synthesis of acylhydrazines and symmetrical and asymmetrical diacylhydrazines from carboxylic acids. This reaction proceeded smoothly under mild conditions and it is quite practical, since the starting carboxylic acids can be easily handled and stored. Cleanliness, simplicity of the method and good to excellent yield of products are other advantages of this method.
Microwave-induced conversion of acid hydrazides to N,N′- diacylhydrazines in solvent-free conditions
Sailu,Komaraiah,Reddy
, p. 1907 - 1910 (2007/10/03)
A new and efficient method of converting acid hydrazides 1 to the corresponding N,N′-diacylhydrazines 2 under microwave irradiation and in solvent-free conditions has been described. Copyright Taylor & Francis Group, LLC.
Oxidation of Hydrazides Using Sodium Perborate: Formation of N,N′-Diacylhydrazines
Jadhav, Vidyadhar K.,Wadagaonkar, Prakash P.,Salunkhe, Manikrao M.
, p. 831 - 833 (2007/10/03)
Substituted aromatic hydrazides react very smoothly with sodium perborate in glacial acetic acid at room temperature to give N,N′-diacylhydrazines in excellent yields and purity.