479054-96-1Relevant articles and documents
Highly efficient method for the synthesis of 1,4-phenylenedithioureas under solvent- and catalyst-free conditions promoted by microwave irridiation
Zhang, Li-Ping,Shang, Xiao-Bo,Wu, Qing-Fen,Zhang, Yang,Li, Jian-Ping
experimental part, p. 1045 - 1052 (2012/02/02)
A highly efficient method for the synthesis of 1,4-phenylenedithioureas promoted by microwave irridiation is reported. It is based on the nucleophilic addition reaction of 1,4-phenylenediisothiocyanate to aromatic amines under solvent- and catalyst-free conditions. The reaction has the advantages of short reaction time, good yields, and environmental acceptability. Taylor & Francis Group, LLC.