55548-96-4Relevant articles and documents
Microwave-promoted, one-pot, solvent-free synthesis of 4-arylcoumarins from 2-hydroxybenzophenones
Crecente-Campo, Jose,Vazquez-Tato, M. Pilar,Seijas, Julio A.
experimental part, p. 4130 - 4135 (2010/09/18)
4-Arylcoumarins are synthesized in very good yields through solvent-free microwave irradiation of 2-hydroxybenzophenones and alkyl malonate in the presence of DBU. The onepot synthesis is carried out with Knoevenagel condensation, intramolecular lactonization, and decarboxylation reactions. The method can be applied to a broad scope of neoflavonoids.