56741-12-9Relevant articles and documents
Solvent-free synthesis of symmetric methylene diestersviadirect reaction of aromatic carboxylates with 1,n-dihaloalkanes
Bai, Lin,Ding, Shenglong,Ma, Xiaofang
, p. 28711 - 28715 (2021/09/22)
An efficient methodology for the synthesis of symmetrical methylene diesters was developed through direct reaction of various aromatic carboxylates with 1,n-dihaloalkanes under solvent-free conditions. This strategy offers a high product yield, facile work-up and purification, and an environmentally friendly approach to obtain long-chain methylene carboxylate scaffolds with increased diversity.
Microwave-assisted, facile, rapid and solvent-free one pot two-component synthesis of some special acylals
Ma, Yu-Heng,Wu, Gang,Jiang, Nan,Ge, Shu-Wang,Zhou, Qian,Sun, Bai-Wang
, p. 81 - 84 (2015/01/30)
A facile, rapid and solvent-free method for the conversion of acids and dihalomethane to the corresponding methylene diesters (acylals) using microwave as activators or assistor, is reported. This method is particularly powerful for the diesterification o
Efficient method for synthesis of methylene diesters using polyethylene glycol as a phase transfer catalyst
Kavitake, Bhanudas P.,Salunkhe, Manikrao M.,Wadgaonkar, Prakash P.
, p. 1703 - 1710 (2007/10/03)
Methylene diesters were synthesized in high yields at room temperature by reacting the potassium salt of a carboxylic acid with dibromo methane under the conditions of solid-liquid phase transfer catalysis using poly (ethylene glycol)-600 (PEG-600) as the
