66190-61-2Relevant articles and documents
A facile method for the synthesis of glaucine and norglaucine from boldine
Huang, Wei-Jan,Chen, Chung-Hsiung,Singh, Om V.,Lee, Su-Lin,Lee, Shoei-Sheng
, p. 3681 - 3686 (2002)
A large-scale preparation of glaucine was achieved by reacting boldine with trimethylphenylammonium chloride and potassium t-butoxide in high yield. Treatment of glaucine with 30% H202, subsequent with hydrated ferrous sulfate, afforded norglaucine in an overall yield of 40%.