70470-10-9Relevant articles and documents
Preparation method of 1,2,3,4,6-O-pentagalloylglucose standard sample
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Paragraph 0031; 0032; 0033; 0034; 0035; 0036; 0037; 0038, (2017/12/05)
The invention discloses a preparation method of a 1,2,3,4,6-O-pentagalloylglucose standard sample. The method comprises the steps that after gallnuat sodium tannic acid is degraded by a methanol acetic acid solution, reduction vaporation is performed to remove an organic solvent, then, diethyl ether and ethyl acetate are used for extraction, ethyl acetate is subjected to partial reduction vaporization to remove an organic solvent, and freeze drying is performed to obtain a crude 1,2,3,4,6-O-pentagalloylglucose product; then, methyl alcohol is used for dissolution, chromatographic separation is performed through sephadex chromatographic columns, the elution portion of 70% acetone is collected, reduction vaporization is performed to remove acetone, a water phase is subjected to freeze drying to obtain the 1,2,3,4,6-O-pentagalloylglucose standard sample. The 1,2,3,4,6-O-pentagalloylglucose standard sample obtained through the method is good in homogeneity, accurate in measurement size and good in stability, and therefore the high-quality standard sample is provided for performing detection, quantification and the like on the content of 1,2,3,4,6-O-pentagalloylglucose.
Complete 1H and 13C NMR assignments of a series of pergalloylated tannins
Lavoie, Serge,Ouellet, Michael,Fleury, Pierre-Yves,Gauthier, Charles,Legault, Jean,Pichette, Andr
, p. 168 - 174 (2016/02/09)
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Plasminogen activator inhibitor-1 inhibitors and methods of use thereof to modulate lipid metabolism
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Page/Page column 61, (2015/09/22)
The invention relates to plasminogen activator-1 (PAI-1) inhibitor compounds and uses thereof in the treatment of any disease or condition associated with elevated PAI-1. The invention includes, but is not limited to, the use of such compounds to modulate lipid metabolism and treat conditions associated with elevated PAI-1, cholesterol, or lipid levels.