736-42-5Relevant articles and documents
Microwave-mediated selective monotetrahydropyranylation of symmetrical diols catalyzed by iodine
Deka,Sarma
, p. 1947 - 1948 (2007/10/03)
Selective protection of one hydroxyl group as its tetrahydropyranyl ether in 1, n-symmetrical diol is achieved by iodine-catalyzed reaction of the diol with dihydropyranyl ether under microwave irradiation.
Highly Selective Monotetrahydropyranylation of Symmetrical Diols Catalysed by a Strongly Acidic Ion-exchange Resin
Nishiguchi, Takeshi,Kuroda, Masahumi,Saitoh, Masahiko,Nishida, Akiko,Fujisaki, Shizuo
, p. 2491 - 2492 (2007/10/03)
Several primary and secondary symmetrical diols, ranging from propane-1,3-diol to decane-1,10-diol, are selectively monoprotected by monotetrahydropyranyl ether formation catalysed by a strongly acidic ion-exchange resin (Dowex 50x x 2, 50-100 mesh) in a 3,4-dihydro-2H-pyran-hydrocarbon mixture.