77129-81-8Relevant articles and documents
Preparation method of phenyl crotonic acid ester compound
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Paragraph 0030-0032; 0036; 0056-0057, (2021/05/19)
The invention relates to the technical field of organic synthesis, in particular to a preparation method of a phenyl crotonate compound, the preparation method comprises the following steps: S1, carrying out Willgerodt-Kindler reaction on an acetophenone
Selective reduction of carbonyl groups in the presence of low-valent titanium reagents
Lin, Wei,Hu, Ming-Hua,Feng, Xian,Fu, Lei,Cao, Cheng-Pao,Huang, Zhi-Bin,Shi, Da-Qing
, p. 2238 - 2242 (2014/04/17)
The chemoselective reduction of several structurally diverse compounds containing carbonyl groups was achieved in the presence of low-valent titanium reagents. This novel synthetic method provides easy access to highly selective reduction of carbonyl groups, and possesses several advantages including one-step procedure, convenient manipulation, good to excellent yields, and short reaction times.
Ultrasound-mediated willgerodt-kindler reactions: Non-thermal synthesis of thioacetamides
Mojtahedi, Mohammad M.,Alishiri, Tooba,Abaee, M. Saeed
experimental part, p. 1910 - 1915 (2011/10/08)
Non-thermal, solvent-free condensation of several aryl methyl ketones with amines and elemental sulfur is efficiently conducted using ultrasonic irradiation within short time periods. Consequently, various thioacetamides are conveniently synthesized. Simi