Engineered co-precipitation chemistry with AMMONIUM CARBONATE (cas 10361-29-2) for scalable synthesis and sintering of improved Sm0.2Ce0.8O1.90 and Gd0.16Pr0.04Ce0.8O1.90 electrolytes for IT-SOFCs
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Add time:08/01/2019 Source:sciencedirect.com
Nanometric powders of doped and co-doped ceria based ceramics with spherical-like morphology and characterized by very low degree of agglomeration, were prepared by using a simple and cheap synthesis route, easily scalable on industrial level, based on an optimized co-precipitation process with AMMONIUM CARBONATE (cas 10361-29-2) as precipitating agent. The as-synthesized powders are completely converted to ceria with fluorite structure. The original morphology and the nanometric features are also preserved. Nearly perfect dense products were obtained after sintering at 1300 °C for 3 h, as by SEM and density measurements. Electrochemical measurements proved that they are all suitable as electrolytes for IT-SOFC.
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