Synthesis and resolution of 2,2-dimethyl-1,3-diphenyl-1,3-propanediol, a new C2-symmetric and conformationally rigid acyclic diol☆
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Add time:09/09/2019 Source:sciencedirect.com
Diastereomerically pure (+)- and (−)-2,2-dimethyl-1,3-diphenyl-1,3-propanediols were synthesized starting from diethyl malonate and resolved through diesters of (−)-camphanic acid and also N-carbethoxy-l-proline. The absolute configuration of the (−)-enantiomer was established by X-ray crystallography.
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