Anantioselective Synthesis of the K-region trans-9,10-Dihydrodiol of Benzo[g]chrysene
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Add time:09/29/2019 Source:infona.pl
Efficient enantioselective syntheses of both enantiomers of the title compound are achieved (>99% ee) via asymmetric dihydroxylation of a stilbene-type precursor using Sharpless catalysts followed by intramolecular biaryl coupling with Pd(PPh 3 ) 2 Cl 2 . This is the first example of direct enantioselective synthesis of a K-region dihydrodiol.
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