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2,6-Dichloronitrobenzene

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Name

2,6-Dichloronitrobenzene

EINECS 210-009-3
CAS No. 601-88-7 Density 1.533 g/cm3
PSA 45.82000 LogP 3.42480
Solubility N/A Melting Point 71 ºC
Formula C6H3 Cl2 N O2 Boiling Point 130ºC
Molecular Weight 192.001 Flash Point 118.9 °C
Transport Information N/A Appearance Powder, alcohol-resistant foam, water spray, carbon dioxide.
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 601-88-7 (2,6-Dichloronitrobenzene) Hazard Symbols ToxicT
Synonyms

1,3-Dichloro-2-nitrobenzene;2,6-Dichloro-1-nitrobenzene; 2,6-Dichloronitrobenzene

Article Data 16

2,6-Dichloronitrobenzene Synthetic route

608-31-1

2,6-Dichloroaniline

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
Stage #1: 2,6-Dichloroaniline With sodium tungstate (VI) dihydrate; sulfuric acid In methanol at 40℃;
Stage #2: With dihydrogen peroxide In methanol; water at 40℃; for 9h; pH=0.5;
Stage #3: With potassium hydroxide In methanol; water at 20 - 40℃; for 2h; Reagent/catalyst; pH-value; Temperature; Solvent;
92%
With sodium perborate In acetic acid at 50 - 55℃;87%
With sodium perborate In acetic acid at 50 - 60℃; for 2h;87%

(2,6-dichlorophenyl)(phenyl)iodonium triflate

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
With sodium nitrite In ethyl acetate at 70℃; for 16h; Temperature; Solvent; Sealed tube; chemoselective reaction;91%
59992-52-8

2,6-dichloro-4-aminonitrobenzene

601-88-7

2,6-dichloronitrobenzene

129825-24-7

2,4-dichloro-3-nitroaniline

601-88-7

2,6-dichloronitrobenzene

5942-05-2

acetic acid-(3,5-dichloro-4-nitro-anilide)

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
With sulfuric acid at 110℃; Kochen des Reaktionsgemisches mit NaNO2 in Aethanol;
541-73-1

1,3-Dichlorobenzene

A

611-06-3

2,4-dichloronitrobenzene

B

618-62-2

3,5-dichloro-1-nitrobenzene

C

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
With Nitrogen dioxide; ozone In dichloromethane at 0 - 5℃; for 1h; Yield given;
With Nitrogen dioxide; ozone In dichloromethane at 0 - 5℃; for 1h; Yield given. Yields of byproduct given;
1194-66-7

2,6-dichloronitrosobenzene

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
With nitric acid Heating;
7697-37-2

nitric acid

541-73-1

1,3-Dichlorobenzene

A

611-06-3

2,4-dichloronitrobenzene

B

601-88-7

2,6-dichloronitrobenzene

31592-84-4

N-(3,5-dichlorophenyl)-acetamide

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nitric acid / die Acetanilide trennt man mit CS2 zersetzt man durch Erhitzen mit konz.Schwefelsaeure
View Scheme
Multi-step reaction with 2 steps
1: Nitrieren; mann trennt das Gemenge durch CS2, worin sich nur 3.5-Dichlor-2-nitro-acetanilid loest, und verseift durch Erhitzen mit konz.Schwefelsaeure
View Scheme
99-09-2

3-nitro-aniline

601-88-7

2,6-dichloronitrobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid; calcium hypochlorite / 40 - 60 °C
View Scheme

2,6-Dichloronitrobenzene Chemical Properties

The molecular formula of 2,6-Dichloronitrobenzene(601-88-7) is C6H3Cl2NO2 and its formula weight is 192.
The density of 2,6-Dichloronitrobenzene(601-88-7) is 1.533 g/cm3  and it has a melting point of  71 °C. The boiling point is  272.9 °C at 760 mmHg . The refractive index is about  1.595 . Its flash point is  118.9 °C .
The chemical synonyms of 2,6-Dichloronitrobenzene(601-88-7) are Benzene, 1,3-dichloro-2-nitro-;2,6-Dichloronitrobenezene;1,3-DICHLORO-3-NITROBENZENE;1,3-Dichloro-2-nitrobenzene;2,6-Dichloronitrobenzene;1-Nitro-2,6-dichlorobenzene
The molecular structure of 2,6-Dichloronitrobenzene(601-88-7):
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