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Cas Database |
| Name |
5-Methoxy-2-methyl-1H-indole |
EINECS | 214-066-5 |
| CAS No. | 1076-74-0 | Density | 1.134 g/cm3 |
| PSA | 25.02000 | LogP | 2.48490 |
| Solubility | N/A | Melting Point |
86-88 °C(lit.) |
| Formula | C10H11NO | Boiling Point | 308.501 °C at 760 mmHg |
| Molecular Weight | 161.203 | Flash Point | 113.125 °C |
| Transport Information | N/A | Appearance | white to light beige crystalline powder |
| Safety | 37/39-26 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
Indole,5-methoxy-2-methyl- (6CI,7CI,8CI);2-Methyl-5-methoxyindole;5-Methoxy-2-methyl-1H-indole;5-Methoxy-2-methylindole;5-Methoxy-2-methyllindole;NSC 63817; |
Article Data | 42 |
5-Methoxy-2-methyl-1H-indole Synthetic route
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With potassium hydroxide In methanol for 1h; Reflux; | 100% |
| With potassium hydroxide In methanol for 1h; Reflux; Large scale; | 98% |
- 104894-18-0
bromure d'acetylamino-2 methoxy-5 benzyltriphenylphosphonium
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With potassium tert-butylate In toluene for 0.25h; Heating; | 97% |
- 98055-12-0
5-methoxy-2-methyl-3-(phenylthio)-1H-indole
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With thiosalicilyc acid In trifluoroacetic acid for 1.5h; Ambient temperature; | 96% |
- 938052-33-6
4-methoxy-2-(prop-1-yn-1-yl)aniline
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With Pd(II)-Y zeolites In toluene at 110℃; for 20h; Catalytic behavior; | 96% |
| With palladium dichloride In acetonitrile at 85℃; Inert atmosphere; |
| Conditions | Yield |
|---|---|
| With acetic acid for 8h; Reagent/catalyst; Reflux; Large scale; | 94% |
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With potassium hydroxide In tetrahydrofuran; ethanol for 6h; Reflux; | 92% |
| With ethanol; potassium hydroxide In tetrahydrofuran Reflux; |
- 153865-35-1
(3-Chloro-4-methoxy-phenyl)-isopropylidene-amine
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With sodium amide; sodium t-butanolate In tetrahydrofuran at 20℃; for 24h; | 87% |
| Conditions | Yield |
|---|---|
| With oxygen; palladium diacetate; acetic acid In dimethyl sulfoxide at 70℃; under 760.051 Torr; for 18h; Schlenk technique; Molecular sieve; | 79% |
| With oxygen; palladium diacetate; acetic acid In dimethyl sulfoxide at 70℃; for 18h; Schlenk technique; Molecular sieve; | 79% |
| With copper diacetate; palladium diacetate In dimethyl sulfoxide at 40℃; for 24h; Inert atmosphere; | 55% |
- 181651-13-8
N-(4-methoxyphenyl)-1-methylethenesulfinamide
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| With boron trifluoride diethyl etherate In dichloromethane at -30℃; for 4h; | 75% |
- 50461-37-5
2-methyl-3-methylthio-5-methoxy-1H-indole
- 1076-74-0
5-methoxy-2-methyl-1H-indole
| Conditions | Yield |
|---|---|
| aluminum nickel | 72% |
5-Methoxy-2-methyl-1H-indole Chemical Properties
IUPAC Name: 5-methoxy-2-methyl-1H-indole
Synonyms of 1H-Indole,5-methoxy-2-methyl- (CAS NO.1076-74-0): EINECS 214-066-5 ; 5-Methoxy-2-methylindole
CAS NO: 1076-74-0
Molecular Formula: C10H11NO
Molecular Weight of 1H-Indole,5-methoxy-2-methyl- (CAS NO.1076-74-0): 161.2004
Molecular Structure:
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H bond acceptors: 2
H bond donors: 1
Freely Rotating Bonds: 1
Polar Surface Area: 14.16 Å2
Index of Refraction: 1.621
Molar Refractivity: 50.03 cm3
Molar Volume: 142.1 cm3
Surface Tension: 43.4 dyne/cm
Density of 1H-Indole,5-methoxy-2-methyl- (CAS NO.1076-74-0): 1.134 g/cm3
Flash Point: 113.1 °C
Enthalpy of Vaporization: 52.73 kJ/mol
Boiling Point: 308.5 °C at 760 mmHg
Vapour Pressure: 0.00123 mmHg at 25°C
Melting point: 86-88 °C
5-Methoxy-2-methyl-1H-indole Safety Profile
Hazard Codes: 
Xi
Risk Statements: 36/37/38
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 37/39-26
S37/39: Wear suitable gloves and eye/face protection.
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
WGK Germany: 3
HazardClass: IRRITANT
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