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Cyclobutylmethylamine
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Name

Cyclobutylmethylamine

 EINECS N/A
CAS No. 4415-83-2 Density 0.889 g/cm3
PSA 26.02000 LogP 1.44550
Solubility N/A Melting Point N/A
Formula C5H11N Boiling Point 90.6 °C at 760 mmHg
Molecular Weight 85.149 Flash Point 2.1 °C
Transport Information N/A Appearance N/A
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 4415-83-2 (Cyclobutylmethylamine) Hazard Symbols N/A
Synonyms

Cyclobutanemethylamine(8CI);(Aminomethyl)cyclobutane;Cyclobutylmethanamine;Cyclobutylmethylamine;

Article Data 7

Cyclobutylmethylamine Synthetic route

4426-11-3

cyclobutanecarbonitrile

4415-83-2

cyclobutylmethylamine

Conditions
ConditionsYield
With hydrogenchloride; palladium on activated charcoal Hydrogenation;
With ethanol; sodium
With borane-THF In tetrahydrofuran Heating;
Stage #1: cyclobutanecarbonitrile With borane In tetrahydrofuran for 17h; Heating / reflux;
Stage #2: With hydrogenchloride In tetrahydrofuran; methanol for 2h; Heating / reflux;
Stage #1: cyclobutanecarbonitrile With hydrogen; acetic acid; platinum(IV) oxide In ethanol under 2689.24 Torr; for 18h;
Stage #2: With sodium hydroxide In diethyl ether; water
59501-58-5

2-aza-bicyclo[2.2.0]hex-5-ene

4415-83-2

cyclobutylmethylamine

Conditions
ConditionsYield
(reduction);
1503-98-6

cyclobutyl amide

4415-83-2

cyclobutylmethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: P2O5 / durch Destillation
2: sodium; alcohol
View Scheme
4415-83-2

cyclobutylmethylamine

C15H17NO3

1-butyl-3-{[(cyclobutylmethyl)amino]methylidene}-8-methylquinoline-2,4(1H,3H)-dione

Conditions
ConditionsYield
With acetic anhydride Reflux;94.6%
75-15-0

carbon disulfide

4415-83-2

cyclobutylmethylamine

13558-70-8

methyl N-(chloroacetyl)carbamate

3-(cyclobutylmethyl)-2-thioxothiazolidin-4-one

Conditions
ConditionsYield
With triethylamine In acetonitrile at 20℃; for 0.166667h;93%
4415-83-2

cyclobutylmethylamine

1416989-68-8

methyl 6-methoxy-3-[({4-[(methylsulfanyl)methyl]-naphthalen-1-yl}carbonyl)amino]pyridine-2-carboxylate

1430228-61-7

N-(cyclobutylmethyl)-6-methoxy-3-({4-[(methylthio)methyl]-1-naphthoyl}amino)-pyridine-2-carboxamide

Conditions
ConditionsYield
With pyridine; dmap In N,N-dimethyl-formamide at 80℃; for 3h;89%
870971-20-3

methyl 6-methoxy-3-{[4-(1H-1,2,3-triazol-1-ylmethyl)-1-naphthoyl]amino}-pyridine-2-carboxylate

4415-83-2

cyclobutylmethylamine

6-methoxy-N-(tetrahydro-2H-pyran-4-ylmethyl)-3-{[4-(lH-1,2,3-triazol-1-ylmethyl)-1-naphthoyl]amino}pyridine-2-carboxamide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 80℃; for 3.83333h;87%
In N,N-dimethyl-formamide at 80℃; for 0.666667h;87%
950661-87-7

2,4-dichloro-7-((2-(trimethylsilyl)ethoxy)methyl)-7H-pyrrolo[2,3-d]pyrimidine-5-carbonitrile

4415-83-2

cyclobutylmethylamine

C18H26ClN5OSi

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In ethanol at 80℃; for 12h;85.5%
870762-08-6

2-(1-naphthalenyl)-1H-pyrido[3,2-d][1,3]oxazin-4-one

4415-83-2

cyclobutylmethylamine

N-(cyclobutylmethyl)-3-[(1-naphthalenylcarbonyl)amino]-2-pyridinecarboxamide

Conditions
ConditionsYield
In methanol; DMF (N,N-dimethyl-formamide) at 20℃; for 18h;83%
In methanol; DMF (N,N-dimethyl-formamide) at 20℃; for 18h;83%
In methanol; N,N-dimethyl-formamide at 0 - 20℃; for 18h;160 mg
4415-83-2

cyclobutylmethylamine

1462-86-8

3-amino-pyridine-2-carboxylic acid

870970-70-0

3-amino-N-(cyclobutylmethyl)pyridine-2-carboxamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; HATU In methanol; DMF (N,N-dimethyl-formamide) at 20℃; for 24h;82%
Stage #1: 3-amino-pyridine-2-carboxylic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.25h;
Stage #2: cyclobutylmethylamine at 20℃; for 1h;		71%
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1 - 2h;28%

Cyclobutylmethylamine Specification

The cas register number of Cyclobutylmethylamine is 4415-83-2. It also can be called as Aminomethylcyclobutane and the Systematic name about this chemical is 1-cyclobutylmethanamine.

Physical properties about Cyclobutylmethylamine are: (1)ACD/LogP: 0.80; (2)#H bond acceptors: 1; (3)#H bond donors: 2; (4)#Freely Rotating Bonds: 2; (5)Polar Surface Area: 3.24Å2; (6)Index of Refraction: 1.469; (7)Molar Refractivity: 26.67 cm3; (8)Molar Volume: 95.7 cm3; (9)Polarizability: 10.57x10-24cm3; (10)Surface Tension: 35.4 dyne/cm; (11)Enthalpy of Vaporization: 33.05 kJ/mol; (12)Boiling Point: 90.6 °C at 760 mmHg; (13)Vapour Pressure: 55.9 mmHg at 25°C .

You can still convert the following datas into molecular structure:
(1)SMILES: NCC1CCC1
(2)InChI: InChI=1/C5H11N/c6-4-5-2-1-3-5/h5H,1-4,6H2
(3)InChIKey: LQNHRNOPWKZUSN-UHFFFAOYAF
(4)Std. InChI: InChI=1S/C5H11N/c6-4-5-2-1-3-5/h5H,1-4,6H2
(5)Std. InChIKey: LQNHRNOPWKZUSN-UHFFFAOYSA-N

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