Tetrahedron Letters p. 5565 - 5568 (1998)
Update date:2022-08-04
Topics:
Nakajima, Noriyuki
Saito, Miho
Ubukata, Makoto
We have succeeded in one-pot preparation of perfluoroimidates at -78 °C by employing the dehydration of perfluoroamide under the 'activated' dimethyl sulfoxide (DMSO) species followed by in situ nitrile trapping with alcohols. MPM and DMPM perfluoroimidates can be used to protect alcohols in place of the trichloroacetimidate with excellent chemical properties and in comparable yields.
View MoreDalian Synco Chemical Co., Ltd.
Contact:+86-411-83635150
Address:Rm 1004, 24, Tangshan Street, Dalian
Guangzhou Reachin Chemical Co., Ltd
Contact:+86-20-37087379 ext.604
Address:A122C-1, Tianyuan Plaza, 401 Tianyuan Rd., Tianhe, Guangzhou, China
Jinan Baozhao Pharmaceutical Co., Ltd
Contact:0086-531-86397156 82371858 82371868
Address:Huaneng Road, Jinan, Shandong ,China
Contact:86-511-85210668 0511-85210668, 85210818, 85210898
Address:Yihai Garden E-902,NO.99 Daxi RD., Zhenjiang Jiiangsu ,China
Xinji City Taida Sinopec Co., Ltd.
Contact:0086-311-85341278
Address:No.6, Nanhua Road,Xinji City Road,Hebei Province,China
Doi:10.1016/S0960-894X(98)00289-3
(1998)Doi:10.1002/jhet.5570350310
(1998)Doi:10.1021/ma60017a012
(1970)Doi:10.1021/jo980800g
(1998)Doi:10.1006/bioo.1998.1082
(1998)Doi:10.1248/cpb.34.2265
(1986)